[1] Karlsruhe Inst Technol, IAM, Hermann von Helmholtz Pl 1, D-76344 Eggenstein Leopoldshafen, Germany
[2] ALBA Synchrotron, Carrer Llum 2-26, Barcelona 08290, Spain
[3] Helmholtz Inst Ulm Electrochem Energy Storage HIU, Albert Einstein Allee 11, D-89081 Ulm, Germany
[4] CSIR CECRI, Electrochem Power Sources Div, Karaikkudi 630003, Tamil Nadu, India