The X-ray structure determination of tert-butylimido methylindane, [CH3In-NC(CH3)(3)](4)

被引:9
作者
Schmid, K [1 ]
Kuhner, S [1 ]
Hausen, HD [1 ]
Weidlein, J [1 ]
机构
[1] UNIV STUTTGART,INST ANORGAN CHEM,D-70569 STUTTGART,GERMANY
来源
ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE | 1997年 / 623卷 / 10期
关键词
methylindium compound; heterocubane; synthesis; X-ray structure;
D O I
10.1002/zaac.19976231004
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
The reaction of MeInCl2 with LiN(H)Bu-t in a 1:2 molar ratio forms [MeIn-(NBu)-Bu-t](4) in high yield, lithium chloride, and the free amine (H2NBu)-Bu-t. The crystal structure of the imidomethylindane with a cubic In4N4 skeleton has been determined.
引用
收藏
页码:1499 / 1500
页数:2
相关论文
共 10 条
  • [1] (C6F5NGAME)4 AND (C6F5NINME)4 - THE 1ST GALLIUM NITROGEN AND INDIUM NITROGEN-COMPOUNDS WITH CUBANE STRUCTURES
    BELGARDT, T
    ROESKY, HW
    NOLTEMEYER, M
    SCHMIDT, HG
    [J]. ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1993, 32 (07): : 1056 - 1058
  • [2] BELGARDT T, 1993, ANGEW CHEM, V105, P1101
  • [3] Two new alkylimido-methylgallanes with cage structure
    Cordeddu, F
    Hausen, HD
    Weidlein, J
    [J]. ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 1996, 622 (03): : 573 - 578
  • [4] SYNTHESIS AND STRUCTURE OF BIS(TRIMETHYLSTANNYL) AND BIS(DIMETHYLHALOSTANNYL) AMINES - THE ROLE OF THE NITROGEN LONE PAIR
    DIEMER, S
    NOTH, H
    POLBORN, K
    STORCH, W
    [J]. CHEMISCHE BERICHTE-RECUEIL, 1992, 125 (02): : 389 - 400
  • [5] HAUSEN HD, 1995, Z NATURFORSCH B, V50, P1419
  • [6] Methyl metal(III)-nitrogen compounds with an oligocyclic as well as cage structures (M(III)=Al,Ga,In)
    Kuhner, S
    Kuhnle, R
    Hausen, HD
    Weidlein, J
    [J]. ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 1997, 623 (01): : 25 - 34
  • [7] KUHNER S, THESIS U STUTTGART
  • [8] Synthesis and characterization of (4-fluorophenyl)amino-based amino- and iminometallanes of group 13. Crystal structures of (MeAlNRf)(4), (MeMNRf)(6).nTHF (M=Al, n=2; M=Ga, n=7), and (MeIn(THF)NRf)(4) (R-f=4-C6H4F)
    Schnitter, C
    Waezsada, SD
    Roesky, HW
    Teichert, M
    Uson, I
    Parisini, E
    [J]. ORGANOMETALLICS, 1997, 16 (06) : 1197 - 1202
  • [9] NITROGEN-COMPOUNDS OF ELEMENTS OF MAIN GROUP-III WITH INTRAMOLECULAR AND INTERMOLECULAR DONOR-ACCEPTOR BONDS .1. SYNTHESES
    VEITH, M
    LANGE, H
    BELO, A
    RECKTENWALD, O
    [J]. CHEMISCHE BERICHTE-RECUEIL, 1985, 118 (04): : 1600 - 1615
  • [10] NITROGEN-COMPOUNDS OF ELEMENTS OF THE 3RD PRINCIPAL GROUP WITH INTRAMOLECULAR AND INTERMOLECULAR DONOR-ACCEPTOR BONDS .2. STRUCTURAL STUDIES
    VEITH, M
    LANGE, H
    RECKTENWALD, O
    FRANK, W
    [J]. JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1985, 294 (03) : 273 - 294