Synthesis of the first unsymmetrical macroheterocycle containing endocyclic phosphorus atoms from pyrocatechol and hydroquinone

被引：1
|
作者：
Blokhin, Yu. I. [1 ]
Kornilov, K. N. [1 ]
Volchenkova, Yu. V. [1 ]
机构：
[1] Moscow State Univ Technol & Management, Moscow 109004, Russia
来源：
RUSSIAN JOURNAL OF GENERAL CHEMISTRY | 2009年 / 79卷 / 02期
关键词：
General Chemistry; Hydroquinone; Macrocycle; Pyrocatechol; Stepwise Mode;
D O I：
10.1134/S1070363209020066
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The first unsymmetrical phosphorus(III)-containing macrocycle having hydroquinone and pyrocatechol fragments, N,N,N',N'-tetraethyl-2,4,11,13-tetraoxa-3,12-diphosphatricyclo[12.2.2.0(5,10)]octadeca-1(16),5,7,9,14,17 hexaene-3,12-diamine, was synthesized in a stepwise mode from hexaethylphosphorous triamide, hydroquinone, and pyrocatechol. The product was converted into the corresponding P,P'-dioxide and P,P'-disulfide.
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页码：200 / 202
页数：3
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