4-Amino-3-(1-naphthyloxymethyl)-1H-1,2,4-triazole-5(4H)-thione

被引：14

作者：

Fun, Hoong-Kun ^{[1
]}

Quah, Ching Kheng ^{[1
]}

Vijesh, A. M. ^{[2
,3
]}

Malladi, Shridhar ^{[3
]}

Isloor, Arun M. ^{[3
]}

机构：

[1] Univ Sains Malaysia, Sch Phys, Xray Crystallog Unit, Usm 11800, Penang, Malaysia

[2] SeQuent Sci Ltd, Ind Area, New Mangalore 575011, Karnataka, India

[3] Natl Inst Technol Karnataka, Dept Chem, Mangalore 575025, India

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷

关键词：

DERIVATIVES;

D O I：

10.1107/S1600536809051368

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C(13)H(12)N(4)OS, the dihedral angle between the triazole and naphthalene ring systems is 67.42 (5)degrees. In the crystal, adjacent molecules are linked via two pairs of intermolecular N-H center dot center dot center dot S interactions, forming R(2)(2)(8) and R(2)(2)(10) ring motifs. Weak C-H center dot center dot center dot S interactions generate infinite chains along [001] and the structure is further consolidated by C-H center dot center dot center dot pi bonds and aromatic pi center dot center dot center dot pi stacking interactions [distance between the centroids of the triazole rings = 3.2479 (7) angstrom].

引用

页码：O29 / U1357

页数：11

共 12 条

[1] Condensed bridgehead nitrogen heterocyclic system: Synthesis and pharmacological activities of 1,2,4-triazolo-[3,4-b]-1,3,4-thiadiazole derivatives of ibuprofen and biphenyl-4-yloxy acetic acid [J].

Amir, Mohd ;

Kumar, Harish ;

Javed, S. A. .

EUROPEAN JOURNAL OF MEDICINAL CHEMISTRY, 2008, 43 (10) :2056-2066

[2] PATTERNS IN HYDROGEN BONDING - FUNCTIONALITY AND GRAPH SET ANALYSIS IN CRYSTALS [J].

BERNSTEIN, J ;

DAVIS, RE ;

SHIMONI, L ;

CHANG, NL .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 1995, 34 (15) :1555-1573

[3]

Bruker, 2005, APEX2 SAINT SADABS

[4] A NITROGEN-GAS-STREAM CRYOSTAT FOR GENERAL X-RAY-DIFFRACTION STUDIES [J].

COSIER, J ;

GLAZER, AM .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1986, 19 (02) :105-107

[5] 4-Amino-3-(o-tolyloxymethyl)-1H-1,2,4-triazole-5(4H)-thione [J].

Fun, Hoong-Kun ;

Liew, Wei-Ching ;

Vijesh, A. M. ;

Padaki, Mahesh ;

Isloor, Arun M. .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 :O1910-U3424

[6] Regioselective reaction: Synthesis, characterization and pharmacological studies of some new Mannich bases derived from 1,2,4-triazoles [J].

Isloor, Arun M. ;

Kalluraya, Balakrishna ;

Shetty, Prashanth .

EUROPEAN JOURNAL OF MEDICINAL CHEMISTRY, 2009, 44 (09) :3784-3787

[7] Synthesis and antioxidant properties of novel N-methyl-1,3,4-thiadiazol-2-amine and 4-methyl-2H-1,2,4-triazole-3(4H)-thione derivatives of benzimidazole class [J].

Kus, Canan ;

Ayhan-Kilcigil, Gulgun ;

Ozbey, Suheyla ;

Kaynak, F. Betuel ;

Kaya, Melek ;

Coban, Tuelay ;

Can-Eke, Benay .

BIOORGANIC & MEDICINAL CHEMISTRY, 2008, 16 (08) :4294-4303

[8] Synthesis and antimicrobial activity of novel sulfone-linked bis heterocycles [J].

Padmavathi, V. ;

Thriveni, P. ;

Reddy, G. Sudhakar ;

Deepti, D. .

EUROPEAN JOURNAL OF MEDICINAL CHEMISTRY, 2008, 43 (05) :917-924

[9] A short history of SHELX [J].

Sheldrick, George M. .

ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122

[10] Structure validation in chemical crystallography [J].

Spek, Anthony L. .

ACTA CRYSTALLOGRAPHICA SECTION D-STRUCTURAL BIOLOGY, 2009, 65 :148-155

← 1 2 →