One-pot synthesis of 3, 4-dihydropyrimidin-2(1H)-ones catalysed by [BMIM]Br under solvent-free condition

被引:0
作者
Rani, J. W. S. [1 ]
Kathing, C. [1 ]
Singh, N. G. [1 ]
Nongrum, R. [1 ]
Rahman, N. [1 ]
Kharmawlong, G. [1 ]
Nongkhlaw, R. [1 ]
机构
[1] North Eastern Hill Univ, Dept Chem, Shillong 793022, Meghalayn, India
来源
BULGARIAN CHEMICAL COMMUNICATIONS | 2017年 / 48卷 / 04期
关键词
3,4-dihydropyrimidin-2(1H)-one; BMIM]Br; solvent-free; multi-component reaction; ADRENOCEPTOR-SELECTIVE ANTAGONISTS; HIGH-YIELDING PROTOCOL; ACIDIC IONIC LIQUID; BIGINELLI REACTION; CONDENSATION REACTION; EFFICIENT SYNTHESIS; REUSABLE CATALYST; MICROWAVE IRRADIATION; 3,4-DIHYDROPYRIMIDIN-2(1H)-ONES; DIHYDROPYRIMIDINONES;
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
One-pot synthesis of 3,4-dihydropyrimidin-2(1H)-ones from beta-ketoester/acetyl acetone, aromatic aldehyde and urea using ionic liquid, [BMIM]Br as an efficient and recyclable catalyst under solvent-free condition is reported in a very simple and environmentally benign method with an efficient yield.
引用
收藏
页码:3 / 10
页数:8
相关论文
共 50 条
  • [21] Citric Acid Catalyzed Synthesis of 3, 4-dihydropyrimidin-2(1H)-ones under Ultrasound Irradiation and Solvent-free Conditions
    Luo, Zhi-Chen
    JOURNAL OF THE CHEMICAL SOCIETY OF PAKISTAN, 2012, 34 (04): : 939 - 941
  • [22] Ammonium chloride-catalyzed one-pot synthesis of 3,4-dihydropyrimidin-2-(1H)-ones under solvent-free conditions
    Shaabani, A
    Bazgir, A
    Teimouri, F
    TETRAHEDRON LETTERS, 2003, 44 (04) : 857 - 859
  • [23] HgCl2 PROMOTED ONE POT SYNTHESIS OF 3, 4-DIHYDROPYRIMIDIN-2 (1H)-ONES AND THIONES UNDER SOLVENT FREE CONDITIONS
    Sachdeva, Harshita
    Saroj, Rekha
    Khaturia, Sarita
    Chauhan, S. S.
    HETEROCYCLIC LETTERS, 2011, 1 (04): : 297 - 304
  • [24] Tetrabutylammonium hydrogen sulfate:: An efficient catalyst for the synthesis of 3,4-dihydropyrimidin-2(1H)-ones under solvent-free conditions
    Shaabani, A
    Bazgir, A
    Arab-Ameri, S
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2004, 179 (11) : 2169 - 2175
  • [25] One-pot synthesis of 3,4-dihydropyrimidin-2(1H)-ones catalyzed by SO3H@imineZCMNPs as a novel, efficient and reusable acidic nanocatalyst under solvent-free conditions
    Abbaspour-Gilandeh, Esmayeel
    Yahyazadeh, Asieh
    Aghaei-Hashjin, Mehraneh
    RSC ADVANCES, 2018, 8 (70) : 40243 - 40251
  • [26] One-pot Synthesis of 3,4-Dihydropyrimidin-2 (1h) -ones Catalyzed by SO3H-Functionalized Mesopolymer under Solvent-free Conditions
    Xing, Rong
    Zhang, Tong
    Zhang, Yue
    ACTA POLYMERICA SINICA, 2014, (05): : 613 - 618
  • [27] Copper(II) tetrafluoroborate as a mild and efficient catalyst for the one-pot synthesis of 3,4-dihydropyrimidin-2(1H)-ones under solvent-free conditions
    Kamal, Ahmed
    Krishnaji, Tadiparthi
    Azhar, Mohd. Ameruddin
    CATALYSIS COMMUNICATIONS, 2007, 8 (12) : 1929 - 1933
  • [28] Tin(IV) catalyzed one-pot synthesis of 3,4-dihydropyrimidin-2-(1H)-ones under solvent-free conditions
    Rameshwar, N.
    Parthasarathy, T.
    RamReddy, A.
    INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 2008, 47 (12): : 1871 - 1875
  • [29] One-pot synthesis of 3,4-dihydropyrimidin-2(1H)-ones catalyzed by acidic ionic liquid
    Ma, Jing-Jun
    Zang, Xiao-Huan
    Zhou, Xin
    Wang, Chun
    Li, Jing-Ci
    Li, Qing
    INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 2007, 46 (12): : 2045 - 2048
  • [30] Samarium chloride catalysed Biginelli reaction:: one-pot synthesis of 3,4-dihydropyrimidin-2(1H)-ones
    Fan, XS
    Zhang, XY
    Zhang, YM
    JOURNAL OF CHEMICAL RESEARCH-S, 2002, (09): : 436 - 438