Synthesis, characterization and thermal analysis of some new transition metal complexes of a polydentate Schiff base

被引：38
作者：
Al-Shihri, AS [1 ]
机构：
[1] King Khalid Univ, Fac Sci, Dept Chem, Abha, Saudi Arabia
来源：
SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY | 2004年 / 60卷 / 05期
关键词：
Schiff bases; transition metals; complexes; IR spectra; thermal analysis;
D O I：
10.1016/j.saa.2003.07.005
中图分类号：
O433 [光谱学];
学科分类号：
0703 ; 070302 ;
摘要：
A new polydentate Schiff base (H3L) was synthesized from the condensation of 2,6-diformyl-4-methyl phenol and S-methylhydrazine-carbodithionate. The 1:1 metal complexes were obtained from the interaction of H3L and the metal ions Cr(III), Co(II), Ni(II), Cu(II), Cd(II) and Hg(II). The complexes were characterized by elemental analysis and IR spectroscopy. Detailed studies of the thermal properties of the complexes were investigated by thermogravimetry techniques. (C) 2003 Elsevier B.V. All rights reserved.
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收藏
页码：1189 / 1192
页数：4
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