Qualitative and quantitative studies of chemical composition of sandarac resin by GC-MS

被引：22
|
作者：
Kononenko, I. [1 ]
de Viguerie, L. [1 ]
Rochut, S. [1 ]
Walter, Ph. [1 ]
机构：
[1] Univ Paris 06, Lab Archeol Mol & Struct, UMR 8220, CNRS, F-75005 Paris, France
来源：
ENVIRONMENTAL SCIENCE AND POLLUTION RESEARCH | 2017年 / 24卷 / 03期
关键词：
Varnish; Sandarac; GC-MS; Diterpenoid; OXIDIZED DITERPENOID ACIDS; MASS-SPECTROMETRY; AGING BEHAVIOR; ART MATERIALS; VARNISHES; IDENTIFICATION; FRESH;
D O I：
10.1007/s11356-016-7261-5
中图分类号：
X [环境科学、安全科学];
学科分类号：
08 ; 0830 ;
摘要：
The chemical composition of sandarac resin was investigated qualitatively and quantitatively by gas chromatography-mass spectrometry (GC-MS). Six compounds with labdane and pimarane skeletons were identified in the resin. The obtained mass spectra were interpreted and the mass spectrometric behaviour of these diterpenoids under EI conditions was described. Quantitative analysis by the method of internal standard revealed that identified diterpenoids represent only 10-30% of the analysed sample. The sandarac resin from different suppliers was analysed (from Kremer, Okhra, Color Rare, La Marchande de Couleurs, L'Atelier Montessori, Hevea). The analysis of different lumps of resins showed that the chemical composition differs from one lump to another, varying mainly in the relative distributions of the components.
引用
收藏
页码：2160 / 2165
页数：6
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