Electrochemical detection of ascorbic acid (vitamin C) using a glassy carbon electrode

被引:29
作者
Ly, SY [1 ]
Chae, JI
Jung, YS
Jung, WW
Lee, HJ
Lee, SH
机构
[1] Seoul Natl Univ Technol, Sch Appl Chem Engn, Dept Fine Chem, Seoul, South Korea
[2] MyGene Biosci Inst, Seoul, South Korea
[3] Gachon Gil Coll, Dept Food & Nutr, Seoul, South Korea
[4] Seoul Natl Univ Technol, Dept Elect & Informat Engn, Seoul, South Korea
来源
NAHRUNG-FOOD | 2004年 / 48卷 / 03期
关键词
anodic stripping voltammetry; ascorbic acid; glass carbon electrode;
D O I
10.1002/food.200300394
中图分类号
TS2 [食品工业];
学科分类号
0832 ;
摘要
A method for the detection of ascorbic acid (AA) was developed using square wave anodic stripping voltammetric (SWASV) analysis with a glassy carbon electrode (GCE). The results indicated a sensitive oxidation peak current of AA on the GCE. A linear curve was obtained within a concentration range of 1-130.0 mug/L with a preconcentration time of 270 s. The relative standard deviation of 30.0 mug/L observed was 0.1016% (n = 12) under optimum conditions. The low detection limit (S/N) was pegged at 0.30 mug/L. Results showed that the method developed can be used to assay biological and pharmaceutical samples, and food samples, as well as other materials requiring AA analyses.
引用
收藏
页码:201 / 204
页数:4
相关论文
共 42 条
[21]  
2-B, 10.1002/1521-3803(20020901)46:5&lt
[22]  
308::AID-FOOD308&gt
[23]  
3.0.CO
[24]  
2-B]
[25]  
Nick H., 1998, J FOOD COMPOS ANAL, V11, P89
[26]  
Oruña-Concha MJ, 1998, J SCI FOOD AGR, V76, P477, DOI [10.1002/(SICI)1097-0010(199803)76:3&lt
[27]  
477::AID-JSFA975&gt
[28]  
3.0.CO
[29]  
2-U, 10.1002/(SICI)1097-0010(199803)76:3<477::AID-JSFA975>3.3.CO
[30]  
2-L]