Synthesis of 6-alkyl carbamato/alkyl thiocarbamato-2,10-dichloro-12-trichloromethyl-12H-dibenzo [d,g][1,3,2]-dioxaphosphocin 6-oxides

被引：1

作者：

Kumar, KA ^{[1
]}

Reddy, CS ^{[1
]}

Reddy, CD ^{[1
]}

机构：

[1] Sri Venkateswara Univ, Dept Chem, Tirupati 517502, Andhra Pradesh, India

来源：

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 2002年 / 177卷 / 6-7期

关键词：

6-alkyl carbamato/alkylthiocarbamato-2,10-dichloro-12-trichloromethyl-12H-dibenzo[d,g][1,3,2]-dioxaphosphocin 6-oxides; IR and NMR (H-1&P-31) spectral analyses;

D O I：

10.1080/10426500212279

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

6-Alkylcarbamato/alkylthiocarbamato-2, 10-dichloro-12-trichloromethyl-12H-dibenzo [d,g][1,3,2]-dioxaphosphocin 6-oxides have been synthesized by the condensation of 2,2-bis(2-hydroxy-5-chlorophenyl)-1,1,1-trichloroethane with dichlorophosphinyl carbamates of different alcohols/thiols in the presence of triethylamine in dry toluene and were characterized by different spectral studies.

引用

页码：1745 / 1748

页数：4

共 8 条

[1]

Corbrjdge D.E.C., 1956, J APPL CHEM, V6, P456

[2] THE INFRA-RED SPECTRA AND CHEMICAL STRUCTURE OF SOME AROMATIC DISULPHIDES, DISULPHONES, AND THIOLSULPHONATES [J].

CYMERMAN, J ;

WILLIS, JB .

JOURNAL OF THE CHEMICAL SOCIETY, 1951, (MAY) :1332-1337

[3]

Fest C., 1982, The Chemistry of Organophosphorus Pesticides

[4]

MIVILLE ME, 1956, Patent No. 2776293

[5] SYNTHESIS OF POTENTIAL DUAL ANTAGONISTS .1. SOME BIS(1-AZIRIDINYL)PHOSPHINYL CARBAMATES AND THEIR STRUCTURAL ANALOGS [J].

PAPANASTASSIOU, ZB ;

BARDOS, TJ .

JOURNAL OF MEDICINAL & PHARMACEUTICAL CHEMISTRY, 1962, 5 (05) :1000-&

[6] CRYSTALLINE 6-COORDINATE PHOSPHORUS-COMPOUNDS DERIVED FROM SPIROPENTAOXYPHOSPHORANES [J].

RAMIREZ, F ;

PRASAD, VAV ;

MARECEK, JF .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1974, 96 (23) :7269-7275

[7] Synthesis of 6-aryloxy- and 6-p-tolylthioxy-2,10-dichloro-12-trichloromethyl-12H-dibenzo[d,g][1,3,2]dioxaphosphocin 6-oxides - X-ray diffraction analyses of 6-(4'-chlorophenoxy)-2,10-dichloro-12-trichloromethyl-12H-dibenzo[d,g][1,3,2]dioxaphosphocin 6-oxide and triethylammonium 2-methylphenyl 2-[{2',2',2'-trichloro-1'-(2''-hydroxyl-5''-chlorophenyl)}ethyl]-4-chlorophenyl phosphate [J].

Reddy, CD ;

Reddy, BS ;

Reddy, PM ;

Berlin, KD ;

Couch, KM ;

Tyagi, S ;

Hossain, MB ;

VanderHelm, D .

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 1996, 115 :149-160

[8]

Thomas L.C., 1974, Interpretation of the Infrared Spectra of Organophosphorus Compounds

← 1 →