Enhanced catalytic reduction of para-nitrophenol using α-MoO3 molybdenum oxide nanorods and stacked nanoplates as catalysts prepared from different precursors

被引:7
作者
Abboudi, Mostafa [1 ,2 ]
Oudghiri-Hassani, Hicham [1 ,3 ]
Al Wadaani, Fahd [1 ]
Rakass, Souad [1 ]
Al Ghamdi, Ali [1 ]
Messali, Mouslim [1 ]
机构
[1] Taibah Univ, Coll Sci, Chem Dept, Almadinah 30002, Saudi Arabia
[2] Univ Abdelmalek Essadi, Fac Sci & Tech Tanger, Dept Genie Chim, BP 416, Tangier, Morocco
[3] Cegep Drummondville, Dept Sci Nat, Drummondville, PQ, Canada
来源
JOURNAL OF TAIBAH UNIVERSITY FOR SCIENCE | 2018年 / 12卷 / 02期
关键词
alpha-MoO3; para-Nitrophenol reduction; nanorods; nanoplates; MOO3; THIN-FILMS; PARTICLE-SIZE; PERFORMANCE; NANOBELTS; DEGRADATION; FABRICATION;
D O I
10.1080/16583655.2018.1451102
中图分类号
O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];
学科分类号
07 ; 0710 ; 09 ;
摘要
Molybdenum oxide, alpha-MoO3, nanorods and stacked nanoplates were prepared from oxalate, citrate and tartrate precursors. These molybdenum oxides showed high efficiencies in the reduction of para-nitrophenol to para-aminophenol in the presence of NaBH4. The prepared precursors were first characterized by thermal gravimetric analysis (TGA) and then thermally decomposed at 350 degrees C (oxalate precursor) and 550 degrees C (citrate and tartrate precursors). The final oxides were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and the Braunauer-Emmet-Teller (BET) technique. The oxalate precursor is the most efficient catalyst for the reduction reaction.
引用
收藏
页码:133 / 137
页数:5
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