Bringing Photochemistry to the Masses: A Simple, Effective, and Inexpensive Photoreactor, Right Out of the Box

被引:25
作者
Aung, Theint [1 ]
Liberko, Charles A. [1 ]
机构
[1] Cornell Coll, Dept Chem, Mt Vernon, IA 52314 USA
关键词
Second-Year Undergraduate; Laboratory Instruction; Organic Chemistry; Laboratory Equipment/Apparatus; Photochemistry; REACTOR; ISOMERIZATION; AZOBENZENE;
D O I
10.1021/ed4000316
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
An inexpensive and commercially available ultraviolet light device, intended for "drying" gel-type fingernail polish, was tested as a photochemical reactor with five organic photochemical laboratory experiments. The device performs satisfactorily and gives product yields comparable to or better than reported results, often in less time. The low cost and ease of use should make photochemical reactions more accessible to undergraduate students.
引用
收藏
页码:939 / 942
页数:4
相关论文
共 31 条
[21]   A photochemical reactor for the study of kinetics and adsorption phenomena [J].
Poce-Fatou, JA ;
Gil, MLA ;
Alcántara, R ;
Botella, C ;
Martín, J .
JOURNAL OF CHEMICAL EDUCATION, 2004, 81 (04) :537-539
[22]   Photochemical dimerization of dibenzylideneacetone - A convenient exercise in [2+2] cycloaddition using chemical ionization mass spectrometry [J].
Rao, G. Nageswara ;
Janardhana, Chelli ;
Ramanathan, V. ;
Rajesh, T. ;
Kumar, P. Harish .
JOURNAL OF CHEMICAL EDUCATION, 2006, 83 (11) :1667-1669
[23]   A SIMPLE PHOTOCHEMICAL EXPERIMENT FOR THE ADVANCED LABORATORY [J].
ROSENFELD, SM .
JOURNAL OF CHEMICAL EDUCATION, 1986, 63 (02) :184-185
[24]  
SCHONBERG A, 1968, PREPARATIVE ORGANIC, P97
[25]  
SCHULTZ AG, 1979, J CHEM EDUC, V56, P555
[26]   A SIMPLE, STUDENT PHOTOCHEMICAL REACTOR [J].
SILBERMAN, R .
JOURNAL OF CHEMICAL EDUCATION, 1970, 47 (02) :122-+
[27]  
Starr J.E., 1964, J CHEM EDUC, V41, P394
[28]   Photochemistry Is Back in the Undergraduate Organic Laboratory [J].
Taber, Douglass F. ;
Paquette, Craig M. .
JOURNAL OF CHEMICAL EDUCATION, 2013, 90 (08) :1105-1106
[29]  
Todd D., 1979, EXPERIMENTAL ORGANIC, P247
[30]   COMBINED PHOTOCHEMISTRY, ORGANIC QUALITATIVE ANALYSIS EXPERIMENT [J].
VANDEMARK, MR ;
KUMLER, PL .
JOURNAL OF CHEMICAL EDUCATION, 1973, 50 (07) :512-514