Crystal growth and characterization of organic single crystal 1-(4-N, N-Dimethylaminopyridinium) acetic acid bromide monohydrate

被引：6

作者：

Lakshmi, K. Udaya ^{[2
]}

Rajesh, N. P. ^{[1
]}

Ramamurthi, K. ^{[3
]}

Varghese, Babu ^{[4
]}

机构：

[1] SSN Coll Engn, Ctr Crystal Growth, Kalavakkam 603110, India

[2] Saveetha Univ, Dept Phys, Coll Engn & Technol, Madras 602105, Tamil Nadu, India

[3] Bharathidasan Univ, Crystal Growth & Thin Film Lab, Sch Phys, Tiruchirappalli 620024, India

[4] Indian Inst Technol, Sophisticated Analyt Instrument Facil, Madras 600036, Tamil Nadu, India

来源：

JOURNAL OF CRYSTAL GROWTH | 2009年 / 311卷 / 08期

关键词：

Crystal structure; X-ray diffraction; Growth from solutions; Single crystal growth; Organic compounds;

D O I：

10.1016/j.jcrysgro.2009.01.142

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

Single crystals of 1-(4-N, N-dimethylaminopyridinium) acetic acid bromide monohydrate were grown by evaporating the solvents from an aqueous solution. The single crystal X-ray structure solution confirmed the monoclinic system of the compound with P2(1)/n space group. The functional groups were identified using FTIR and Laser Raman. Proton NMR spectral analyses were carried out to identify the position of protons. Optical properties like second harmonic generation, UV-Vis in transmittance mode and fluorescence were studied. Thermogravimetrical analysis was carried out to determine the thermal properties of the grown crystal. (c) 2009 Elsevier B.V. All rights reserved.

引用

页码：2484 / 2489

页数：6

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