A simple color concentration measurement technique for powders

被引:20
作者
Emady, Heather N. [1 ,2 ]
Wittman, Maya [2 ]
Koynov, Sara [2 ]
Borghard, William G. [2 ]
Muzzio, Fernando J. [2 ]
Glasser, Benjamin J. [2 ]
Cuitino, Alberto M. [3 ]
机构
[1] Arizona State Univ, Sch Engn Matter Transport & Energy, Tempe, AZ 85287 USA
[2] Rutgers State Univ, Dept Chem & Biochem Engn, Piscataway, NJ 08854 USA
[3] Rutgers State Univ, Dept Mech & Aerosp Engn, Piscataway, NJ 08854 USA
关键词
Spectrophotometer; Tracer; Mixing; Color; Powder; Calibration; RESIDENCE TIME DISTRIBUTION; AXIAL-DISPERSION; MIXTURES; QUALITY; FOOD; FLOW; RTD;
D O I
10.1016/j.powtec.2015.07.050
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
Looking for a way to measure residence time distributions of an 80 micron fluidized cracking catalyst (FCC) powder, a simple measurement technique was discovered that quantifies tracer color concentration. Using a color spectrophotometer that measures percent reflectance as a function of wavelength, a calibration curve can be constructed for standard mixtures of dyed and un-dyed powder. This calibration curve can then be used to determine the color concentration of an unknown sample by measuring its reflectance. The effects of operating parameters such as dye strength, aperture size, surface roughness, sample volume and depth, and continuous flow were all evaluated. This spectrophotometric technique was found to be a quick and simple way to measure colored mixture concentrations. In addition to being ideal for residence time distribution applications, it has the potential to easily quantify mixing in any unit operation, batch or continuous. (C) 2015 Elsevier B.V. All rights reserved.
引用
收藏
页码:392 / 400
页数:9
相关论文
共 23 条
[1]   Polymer powders mixing part II: Multi-component mixing dynamics using RGB color analysis [J].
Aissa, Amara Ait ;
Duchesne, Carl ;
Rodrigue, Denis .
CHEMICAL ENGINEERING SCIENCE, 2010, 65 (12) :3729-3738
[2]   Pharmaceutical dry powder blending and scale-up: Maintaining equivalent mixing conditions using a coloured tracer powder [J].
Barling, David ;
Morton, David A. V. ;
Hapgood, Karen .
POWDER TECHNOLOGY, 2015, 270 :461-469
[3]   Principal component analysis for characterising homogeneity in powder mixing using image processing techniques [J].
Berthiaux, H ;
Mosorov, V ;
Tomczak, L ;
Gatumel, C ;
Demeyre, U .
CHEMICAL ENGINEERING AND PROCESSING-PROCESS INTENSIFICATION, 2006, 45 (05) :397-403
[4]   Discrete element method simulation of a conical screen mill: A continuous dry coating device [J].
Deng, Xiaoliang ;
Scicolone, James ;
Han, Xi ;
Dave, Rajesh N. .
CHEMICAL ENGINEERING SCIENCE, 2015, 125 :58-74
[5]   Measurement of Residence Time Distribution in a Rotary Calciner [J].
Gao, Yijie ;
Glasser, Benjamin J. ;
Ierapetritou, Marianthi G. ;
Cuitino, Alberto ;
Muzzio, Fernando J. ;
Beeckman, Jean W. ;
Fassbender, Natalie A. ;
Borghard, William G. .
AICHE JOURNAL, 2013, 59 (11) :4068-4076
[6]   A review of the Residence Time Distribution (RTD) applications in solid unit operations [J].
Gao, Yijie ;
Muzzio, Fernando J. ;
Ierapetritou, Marianthi G. .
POWDER TECHNOLOGY, 2012, 228 :416-423
[7]   Characterizing continuous powder mixing using residence time distribution [J].
Gao, Yijie ;
Vanarase, Aditya ;
Muzzio, Fernando ;
Ierapetritou, Marianthi .
CHEMICAL ENGINEERING SCIENCE, 2011, 66 (03) :417-425
[8]   A calibration procedure to obtain solid concentrations from digital images of bulk powders [J].
Grasa, G ;
Abanades, JC .
POWDER TECHNOLOGY, 2001, 114 (1-3) :125-128
[9]   The influence of the riser exit on the particle residence time distribution in a circulating fluidised bed riser [J].
Harris, AT ;
Davidson, JF ;
Thorpe, RB .
CHEMICAL ENGINEERING SCIENCE, 2003, 58 (16) :3669-3680
[10]   Particle residence time distributions in circulating fluidised beds [J].
Harris, AT ;
Davidson, JF ;
Thorpe, RB .
CHEMICAL ENGINEERING SCIENCE, 2003, 58 (11) :2181-2202