2-Chloromethyl-2,3-dihydrothieno[3,4-b][1,4]dioxine

被引：3

作者：

Xu, Jian ^{[1
]}

Xu, Hao ^{[1
]}

Quan, Ji-cai ^{[1
]}

Sha, Fei ^{[1
]}

Yao, Cheng ^{[1
]}

机构：

[1] Nanjing Univ Technol, Coll Sci, Nanjing 210009, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2009年 / 65卷

关键词：

D O I：

10.1107/S1600536809007156

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the molecule of the title compound, C7H7ClO2S, the six-membered ring adopts a twisted conformation. In the crystal structure, weak intermolecular C-H center dot center dot center dot O hydrogen bonds link the molecules. There is also a weak C-H center dot center dot center dot pi interaction.

引用

页码：O668 / U1256

页数：9

共 9 条

[1] TABLES OF BOND LENGTHS DETERMINED BY X-RAY AND NEUTRON-DIFFRACTION .1. BOND LENGTHS IN ORGANIC-COMPOUNDS [J].

ALLEN, FH ;

KENNARD, O ;

WATSON, DG ;

BRAMMER, L ;

ORPEN, AG ;

TAYLOR, R .

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1987, (12) :S1-S19

[2] GENERAL DEFINITION OF RING PUCKERING COORDINATES [J].

CREMER, D ;

POPLE, JA .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1975, 97 (06) :1354-1358

[3]

Enraf-Nonius, 1989, CAD 4 SOFTW

[4]

Farrujia LJ., 1997, J APPL CRYSTALLOGR, V30, P565, DOI [10.1107/S0021889897003117, DOI 10.1107/S0021889897003117]

[5]

Harms K., 1995, XCAD4

[6]

JOSE LS, 2005, ORG LETT, V7, P2345

[7] A SEMI-EMPIRICAL METHOD OF ABSORPTION CORRECTION [J].

NORTH, ACT ;

PHILLIPS, DC ;

MATHEWS, FS .

ACTA CRYSTALLOGRAPHICA SECTION A-CRYSTAL PHYSICS DIFFRACTION THEORETICAL AND GENERAL CRYSTALLOGRAPHY, 1968, A 24 :351-&

[8] A short history of SHELX [J].

Sheldrick, George M. .

ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122

[9] Structure validation in chemical crystallography [J].

Spek, Anthony L. .

ACTA CRYSTALLOGRAPHICA SECTION D-STRUCTURAL BIOLOGY, 2009, 65 :148-155

← 1 →