The NIR determination of ascorbic acid in pharmaceuticals

被引:0
作者
Zalewska, Malgorzata
Olszanowski, Andrzej
Dlugosz, Monika
机构
[1] Politechn Poznanska, Inst Inzynierii & Technol Chem, PL-60965 Poznan, Poland
[2] GlaxoSmithKline Pharmaceut SA, Poznan, Poland
来源
PRZEMYSL CHEMICZNY | 2006年 / 85卷 / 8-9期
关键词
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The 10,000-4,000 cm(-1) spectra recorded in the reflectance mode were used to detect and det. ascorbic acid in intact tablets of 5 com. prepns. The NIR data compared well with those found by TLC and potentiometric iodometry used as the ret. methods. Full qual. and quant. assay took 30 min, a test time acceptable for large-lot production. Each app. to be used in series measurements requires an individual quant procedure.
引用
收藏
页码:691 / 694
页数:4
相关论文
共 50 条
[31]   DETERMINATION OF GOLD WITH ASCORBIC ACID [J].
STATHIS, EC ;
GATOS, HC .
INDUSTRIAL AND ENGINEERING CHEMISTRY-ANALYTICAL EDITION, 1946, 18 (12) :801-801
[32]   COMPLEXOMETRIC DETERMINATION OF ASCORBIC ACID [J].
PRZYBOROWSKI, L .
DISSERTATIONES PHARMACEUTICAE ET PHARMACOLOGICAE, 1966, 18 (05) :505-+
[33]   ELECTROMETRIC DETERMINATION OF ASCORBIC ACID [J].
LIEBMANN, H ;
AYRES, AD .
ANALYST, 1945, 70 (836) :411-413
[34]   Colorimetric determination of ascorbic acid [J].
Scudi, JV ;
Ratish, HD .
INDUSTRIAL AND ENGINEERING CHEMISTRY-ANALYTICAL EDITION, 1939, 11 :0098-0098
[35]   ESTIMATION OF ASCORBIC ACID IN PHARMACEUTICALS WITH PARTICULAR REFERENCE TO INTERFERING SUBSTANCES [J].
CHAPMAN, DG ;
ROCHON, O ;
CAMPBELL, JA .
ANALYTICAL CHEMISTRY, 1951, 23 (08) :1113-1115
[36]   DETERMINATION OF ASCORBIC-ACID IN BODY-FLUIDS, FOODSTUFFS, AND PHARMACEUTICALS BY LIQUID-CHROMATOGRAPHY WITH ELECTROCHEMICAL DETECTION [J].
PACHLA, LA ;
KISSINGER, PT .
ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1975, 170 (AUG24) :42-42
[37]   Spectrophotometric Determination of L-Ascorbic Acid in Pharmaceuticals Based on Its Oxidation by Potassium Peroxymonosulfate and Hydrogen Peroxide [J].
Salkic, Mirsad ;
Selimovic, Amra .
CROATICA CHEMICA ACTA, 2015, 88 (01) :73-79
[38]   DETERMINATION OF ASCORBIC-ACID IN FOODSTUFFS, PHARMACEUTICALS, AND BODY-FLUIDS BY LIQUID-CHROMATOGRAPHY WITH ELECTROCHEMICAL DETECTION [J].
PACHLA, LA ;
KISSINGER, PT .
ANALYTICAL CHEMISTRY, 1976, 48 (02) :364-367
[39]   Colorimetric determination of ascorbic acid in pharmaceuticals using UVI-4-(2-pyridylazo)resorcinol complex [J].
Arya, SP ;
Jain, P .
JOURNAL OF THE INDIAN CHEMICAL SOCIETY, 2002, 79 (01) :95-96
[40]   USE OF OXALIC ACID IN THE DETERMINATION OF ASCORBIC ACID [J].
HUELIN, FE .
ANALYST, 1950, 75 (892) :391-392