Headspace single-drop microextration for the detection of organotin compounds

被引：98

作者：

Colombini, V ^{[1
]}

Bancon-Montigny, C ^{[1
]}

Yang, L ^{[1
]}

Maxwell, P ^{[1
]}

Sturgeon, RE ^{[1
]}

Mester, Z ^{[1
]}

机构：

[1] Natl Res Council Canada, Inst Natl Measurement Stand, Ottawa, ON K1A 0R6, Canada

来源：

TALANTA | 2004年 / 63卷 / 03期

关键词：

liquid-liquid extraction; gas chromatography; supercritical fluid extraction;

D O I：

10.1016/j.talanta.2003.11.035

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

The performance of single-drop microextraction (SDME), coupled with gas chromatography/mass spectrometry, was assessed for the determination of tributyltin compounds in water and solid samples. Experimental parameters impacting the performance of SDME, such as microextraction solvent and sampling and stirring time, were investigated. Analytical results obtained by SDME were compared with those generated by conventional solid phase microextraction (SPME) and liquid-liquid extraction (LLE) for the determination of TBT in PACS-2 sediment certified reference material (CRM). (C) 2003 Elsevier B.V. All rights reserved.

引用

页码：555 / 560

页数：6

共 30 条

[1] ARNALDO CA, 1995, ANAL CHEM, V67, P2562
[2] Improvement of measurement precision of SPME-GC/MS determination of tributyltin using isotope dilution calibration
Bancon-Montigny, C
Maxwell, P
Yang, L
Mester, Z
Sturgeon, RE
[J]. ANALYTICAL CHEMISTRY, 2002, 74 (21) : 5606 - 5613
[3] Solid phase extraction of trace elements
Camel, V
[J]. SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY, 2003, 58 (07) : 1177 - 1233
[4] Speciation of butyltin compounds in marine sediments with headspace solid phase microextraction and gas chromatography-mass spectrometry
Cardellicchio, N
Giandomenico, S
Decataldo, A
Di Leo, A
[J]. FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY, 2001, 369 (06): : 510 - 515
[5] Application of solvent microextraction to the analysis of amphetamines and phencyclidine in urine
Casari, C
Andrews, ARJ
[J]. FORENSIC SCIENCE INTERNATIONAL, 2001, 120 (03) : 165 - 171
[6] Determination of arsenic by electrothermal atomic absorption spectrometry using headspace liquid phase microextraction after in situ hydride generation
Chamsaz, M
Arbab-Zavar, MH
Nazari, S
[J]. JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY, 2003, 18 (10) : 1279 - 1282
[7] Development of a screening method for cocaine and cocaine metabolites in urine using solvent microextraction in conjunction with gas chromatography
de Jager, LS
Andrews, ARJ
[J]. JOURNAL OF CHROMATOGRAPHY A, 2001, 911 (01) : 97 - 105
[8] Development of a rapid screening technique for organochlorine pesticides using solvent microextraction (SME) and fast gas chromatography (GC)
de Jager, LS
Andrews, ARJ
[J]. ANALYST, 2000, 125 (11) : 1943 - 1948
[9] Solid-phase micro-extraction in bioanalysis, exemplified by lidocaine determination
de Jong, GJ
Koster, EHM
[J]. CHROMATOGRAPHIA, 2000, 52 (Suppl 1) : S12 - S13
[10] Recovery, enrichment and selectivity in liquid-phase microextraction - Comparison with conventional liquid-liquid extraction
Ho, TS
Pedersen-Bjergaard, S
Rasmussen, KE
[J]. JOURNAL OF CHROMATOGRAPHY A, 2002, 963 (1-2) : 3 - 17

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