Facile preparation of nanosized yttrium oxide by the thermal decomposition of amorphous Schiff base yttrium complex precursor

被引：9

作者：

Pizl, Martin ^{[1
]}

Jankovsky, Ondrej ^{[1
]}

Ulbrich, Pavel ^{[2
]}

Szabo, Norbert ^{[1
]}

Hoskovcova, Irena ^{[1
]}

Sedmidubsky, David ^{[1
]}

Bartunek, Vilem ^{[1
]}

机构：

[1] Univ Chem & Technol Prague, Fac Chem Technol, Dept Inorgan Chem, Tech 5, Prague 16628 6, Czech Republic

[2] Univ Chem & Technol Prague, Fac Food & Biochem Technol, Dept Biochem & Microbiol, Tech 3, Prague 16628 6, Czech Republic

来源：

JOURNAL OF ORGANOMETALLIC CHEMISTRY | 2017年 / 830卷

关键词：

Non-linear optics; Nanoparticles; Y2O3; Schiff base; Thermal decomposition; Rare earths; LANTHANIDE COMPLEXES; Y2O3; NANOPARTICLES; LUMINESCENCE; TEMPERATURE; PYRIDOXAL; Y(OH)(3);

D O I：

10.1016/j.jorganchem.2016.12.018

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Nanoparticles of yttrium (III) oxide were synthetized by thermal combustion of previously prepared yttrium complex of pyridoxylidenealanine under air atmosphere at 750 degrees C Amorphous complex was characterized by XRD and IR and NMR spectroscopy. The prepared nanoparticles were characterized by XRD and TEM revealing the size of the vast majority of particles ranging from 10 to 30 nm. The synthesis method can be modified by addition of any RE and can be used for many applications especially in the field of non-linear optics or in biomedical applications where use of more fine nanoparticles may be problematic or even dangerous. (C) 2016 Elsevier B.V. All rights reserved.

引用

收藏

页码：146 / 149

页数：4

相关论文

共 16 条

[1] Cathodic electrodeposition of Y(OH)3 and Y2O3 nanostructures from chloride bath. Part II: Effect of the bath temperature on the crystal structure, composition and morphology [J].

Aghazadeh, Mustafa ;

Barmi, Abbas-Ali Malek ;

Shiri, Hamid Mohammad ;

Sedaghat, Sajjad .

CERAMICS INTERNATIONAL, 2013, 39 (02) :1045-1055

[2] Low-temperature electrochemical synthesis and characterization of ultrafine Y(OH)3 and Y2O3 nanoparticles [J].

Aghazadeh, Mustafa ;

Yousefi, Taher ;

Ghaemi, Mehdi .

JOURNAL OF RARE EARTHS, 2012, 30 (03) :236-240

[3] Tunable rapid microwave synthesis of up-converting hexagonal NaYxGdyYbzEr(1-x-y-z)F4 nanocrystals in large quantity [J].

Bartunek, Vilem ;

Pinc, Jan ;

Ulbrich, Pavel ;

Rak, Jakub ;

Pelankova, Barbora ;

Kral, Vladimir ;

Kuchar, Martin ;

Jezek, Petr ;

Engstova, Hana ;

Smolkova, Katarina .

JOURNAL OF FLUORINE CHEMISTRY, 2015, 178 :56-60

[4] Annealing effects on structural and luminescence properties of red Eu3+-doped Y2O3 nanophosphors prepared by sol-gel method [J].

Boukerika, A. ;

Guerbous, L. .

JOURNAL OF LUMINESCENCE, 2014, 145 :148-153

[5] Preparation and photodynamic therapy application of NaYF4:Yb, Tm-NaYF4:Yb, Er multifunctional upconverting nanoparticles [J].

Chen, Xiaolan ;

Zhao, Zengxia ;

Jiang, Mengying ;

Que, Daiping ;

Shi, Saige ;

Zheng, Nanfeng .

NEW JOURNAL OF CHEMISTRY, 2013, 37 (06) :1782-1788

[6] Interligand CH center dot center dot center dot pi interaction in binary cobalt(III) complexes of N-pyridoxy-L-amino acids. Biological significance of the pyridoxal 2-methyl group [J].

Jitsukawa, K ;

Iwai, K ;

Masuda, H ;

Ogoshi, H ;

Einaga, H .

JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1997, (20) :3691-3698

[7] Biopolymer-assisted synthesis of yttrium oxide nanoparticles [J].

Kaygusuz, Hakan ;

Bilir, Gokhan ;

Tezcan, Filiz ;

Erim, F. Bedia ;

Ozen, Gonul .

PARTICUOLOGY, 2014, 14 :19-23

[8] Synthesis, spectroscopic characterization and antibacterial studies of lanthanide(III) Schiff base complexes containing N, O donor atoms [J].

Lekha, L. ;

Raja, K. Kanmani ;

Rajagopal, G. ;

Easwaramoorthy, D. .

JOURNAL OF MOLECULAR STRUCTURE, 2014, 1056 :307-313

[9] Preparation of Y2O3:Er,Yb nanoparticles by laser ablation in liquid [J].

Nunokawa, Takashi ;

Onodera, Yuji ;

Hara, Masahiko ;

Kitamoto, Yoshitaka ;

Odawara, Osamu ;

Wada, Hiroyuki .

APPLIED SURFACE SCIENCE, 2012, 261 :118-122

[10] Luminescence and structural properties of lanthanide complexes of Schiff bases derived from pyridoxal and amino acids [J].

Puntus, Lada ;

Zhuravlev, Konstantin ;

Lyssenko, Konstantin ;

Antipin, Mikhail ;

Pekareva, Irina .

DALTON TRANSACTIONS, 2007, (36) :4079-4088