Determination of Organic Acids in Tissues and Exudates of Maize, Lupin, and Chickpea by High-Performance Liquid Chromatography-Tandem Mass Spectrometry

被引：24
|
作者：
Erro, Javier [1 ]
Zamarreno, Angel M. [2 ]
Yvin, Jean-Claude [2 ]
Garcia-Mina, Jose M. [1 ,2 ]
机构：
[1] Univ Navarra, Dept Chem & Soil Chem, E-31080 Pamplona, Spain
[2] CIPAV Poligono Arazuri Orcoyen, R&D AFI Roullier Grp, Orcoyen 31160, Spain
来源：
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY | 2009年 / 57卷 / 10期
关键词：
ESI-MS/MS; ion-exclusion chromatography; organic acids determination; maize; lupin; chickpea; ION-EXCLUSION CHROMATOGRAPHY; ALIPHATIC CARBOXYLIC-ACIDS; GAS-CHROMATOGRAPHY; CAPILLARY-ELECTROPHORESIS; ELECTROCHEMICAL DETECTION; DICARBOXYLIC-ACIDS; RHIZOSPHERE; MOBILIZATION; SEPARATION; QUANTIFICATION;
D O I：
10.1021/jf804003v
中图分类号：
S [农业科学];
学科分类号：
09 ;
摘要：
This article describes a fast and simple methodology for the extraction and determination of organic acids in tissues and root exudates of maize, lupin, and chickpea by LC/MS/MS. Its main advantage is that it does not require sample prepurification before HPLC analysis or sample derivatization to improve sensibility. The results obtained showed good precision and accuracy, a recovery close to 100%, and no significant matrix effect. Moreover, the sensibility of the method is in general better than that of previously described methodologies, with detection limits between 15 and 900 pg injected.
引用
收藏
页码：4004 / 4010
页数：7
相关论文
共 50 条
  • [41] Determination of Drugs in Plasma Samples by High-Performance Liquid Chromatography-Tandem Mass Spectrometry for Therapeutic Drug Monitoring of Schizophrenic Patients
    Domingues, Diego Soares
    Lemos Pinto, Monia Aparecida
    de Souza, Israel Donizeti
    Cecilio Hallak, Jaime Eduardo
    de Souza Crippa, Jose Alexandre
    Costa Queiroz, Maria Eugenia
    JOURNAL OF ANALYTICAL TOXICOLOGY, 2016, 40 (01) : 28 - 36
  • [42] Concurrent determination of cyanide and thiocyanate in human and swine antemortem and postmortem blood by high-performance liquid chromatography-tandem mass spectrometry
    Alluhayb, Abdullah H.
    Severance, Carter
    Hendry-Hofer, Tara
    Bebarta, Vikhyat S.
    Logue, Brian A.
    ANALYTICAL AND BIOANALYTICAL CHEMISTRY, 2023, 415 (26) : 6595 - 6609
  • [43] Determination of pesticide residues in wine by membrane-assisted solvent extraction and high-performance liquid chromatography-tandem mass spectrometry
    Moeder, M.
    Bauer, C.
    Popp, P.
    van Pinxteren, M.
    Reemtsma, T.
    ANALYTICAL AND BIOANALYTICAL CHEMISTRY, 2012, 403 (06) : 1731 - 1741
  • [44] Class-specific molecularly imprinted polymers for the selective extraction and determination of sulfonylurea herbicides in maize samples by high-performance liquid chromatography-tandem mass spectrometry
    She, Yong-xin
    Cao, Wei-qiang
    Shi, Xiao-mei
    Lv, Xiao-ling
    Liu, Jia-jia
    Wang, Rong-yan
    Jin, Fen
    Wang, Jing
    Xiao, Hang
    JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES, 2010, 878 (23): : 2047 - 2053
  • [45] Determination of organic acids in fruits and vegetables by liquid chromatography with tandem-mass spectrometry
    Flores, Pilar
    Hellin, Pilar
    Fenoll, Jose
    FOOD CHEMISTRY, 2012, 132 (02) : 1049 - 1054
  • [46] Development of a liquid chromatography-tandem mass spectrometry with pressurized liquid extraction for determination of glucocorticoid residues in edible tissues
    Chen, Dongmei
    Tao, Yanfei
    Liu, Zhaoying
    Zhang, Huahai
    Liu, Zhenli
    Wang, Yulian
    Huang, Lingli
    Pan, Yuanhu
    Peng, Dapeng
    Dai, Menghong
    Wang, Xu
    Yuan, Zonghui
    JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES, 2011, 879 (02): : 174 - 180
  • [47] Determination of 13 Organic Toxicants in Human Blood by Liquid-Liquid Extraction Coupling High-Performance Liquid Chromatography Tandem Mass Spectrometry
    Song, Aiying
    ANALYTICAL SCIENCES, 2016, 32 (06) : 645 - 651
  • [48] Online Liquid Chromatography-Tandem Mass Spectrometry Cyanide Determination in Blood
    Lacroix, C.
    Saussereau, E.
    Boulanger, F.
    Goulle, J. P.
    JOURNAL OF ANALYTICAL TOXICOLOGY, 2011, 35 (03) : 143 - 147
  • [49] Determination of voriconazole in human plasma by liquid chromatography-tandem mass spectrometry
    Teng, G-Sh.
    Zhao, L. -Z.
    Li, X.
    BULGARIAN CHEMICAL COMMUNICATIONS, 2016, 48 (01): : 147 - 152
  • [50] Determination of five quaternary ammonium compounds in foodstuffs using high performance liquid chromatography-tandem mass spectrometry
    Cao, Haiwei
    Kang, Mingqin
    Chen, Zhen
    Li, Ling
    Cui, Minghui
    Chen, Mingyan
    Zhang, Hanqi
    Wang, Yinghua
    ANALYTICAL METHODS, 2014, 6 (13) : 4790 - 4796
12345