Characterization of pure and doped potassium hydrogen tartrate single crystals grown in silica gel

被引：18
|
作者：
Quasim, I. [1 ]
Firdous, A. [2 ]
Sahni, N. [3 ]
Khosa, S. K. [1 ]
Kotru, P. N. [1 ]
机构：
[1] Univ Jammu, Dept Phys & Elect, Crystal Growth & Mat Res Lab, Jammu 180006, India
[2] Natl Inst Technol, Dept Phys, Kashmir 190006, Jammu & Kashmir, India
[3] Panjab Univ, Dept Geol, Chandigarh 160014, India
来源：
CRYSTAL RESEARCH AND TECHNOLOGY | 2009年 / 44卷 / 05期
关键词：
gel technique; doped potassium hydrogen tartrate; SEM; XRD; CH analysis; FTIR spectroscopy; TGA;
D O I：
10.1002/crat.200800617
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
Growth of pure-, sodium- and lithium- doped potassium hydrogen tartrate single crystals by gel technique is reported. Growth conditions conducive for the growth of single crystals are worked out. The crystals are characterized by using powder XRD, SEM, FTIR, AES, EDAX, CH analysis and thermoanalytical techniques. The stoichiometric composition for the grown crystals are established as KHC4H4O6 center dot H2O, (K)(0.98)(Na)(0.02)HC4H4O6 center dot H2O and (K)(0.94)(Li)(0.06)HC4H4O6 center dot H2O. Doping of sodium and lithium in the pure potassium hydrogen tartrate single crystals is found to influence the size, perfection, morphology, crystal structure and the thermal stability of crystals. (C) 2009 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim
引用
收藏
页码：539 / 547
页数：9
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