Solid state linear-dichroic infrared (IR-LD) spectroscopic characterization of α- and β-glycine polymorphs

被引：12
作者：
Ivanova, Bojidarka B. [1 ]
机构：
[1] Univ Sofia, Dept Chem, Sofia 1164, Bulgaria
来源：
CENTRAL EUROPEAN JOURNAL OF CHEMISTRY | 2006年 / 4卷 / 01期
关键词：
alpha- and beta-glycine polymorphs; solid state IR-LD analysis;
D O I：
10.1007/s11532-005-0008-7
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
IR-LD spectroscopic analysis using nematic liquid crystal suspension as a solid-state orientation technique and the reducing- difference procedure for polarized spectra interpretation are applied to the alpha- and beta-polymorphs of glycine. Both structural analysis and detailed IR band assignments were carried out. (C) Central European Science Journals Warsaw and Springer-Verlag Berlin Heidelberg. All rights reserved.
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页码：111 / 117
页数：7
相关论文
共 22 条
[1]   HYDROGEN-BOND STUDIES .77. ELECTRON-DENSITY DISTRIBUTION IN ALPHA-GLYCINE - X-N DIFFERENCE FOURIER SYNTHESIS VS AB-INITIO CALCULATIONS [J].
ALMLOF, J ;
KVICK, A ;
THOMAS, JO .
JOURNAL OF CHEMICAL PHYSICS, 1973, 59 (08) :3901-3906
[2]  
[Anonymous], SPECTROSCOPY POLARIZ
[3]   A solid-state linear dichroic infrared spectral study of 4-aminopyridine [J].
Arnaudov, MG ;
Ivanova, BB ;
Dinkov, SG .
VIBRATIONAL SPECTROSCOPY, 2005, 37 (01) :145-147
[4]   Polarised IR and Raman spectra of the γ-glycine single crystal [J].
Baran, J ;
Ratajczak, H .
SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 2005, 61 (07) :1611-1626
[5]   Variable-temperature and variable-pressure studies of small-molecule organic crystals [J].
Boldyreva, EV ;
Drebushchak, TN ;
Shakhtshneider, TP ;
Sowa, H ;
Ahsbahs, H ;
Goryainov, SV ;
Ivashevskaya, SN ;
Kolesnik, EN ;
Drebushchak, VA ;
Burgina, EB .
ARKIVOC, 2004, :128-155
[6]   Structural distortion of the α, β, and γ polymorphs of glycine on cooling [J].
Boldyreva, EV ;
Drebushchak, TN ;
Shutova, ES .
ZEITSCHRIFT FUR KRISTALLOGRAPHIE, 2003, 218 (05) :366-376
[7]   β-glycine [J].
Drebushchak, TN ;
Boldyreva, EV ;
Shutova, ES .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2002, 58 :O634-O636
[8]   Crystallization in polymorphic systems:: The solution-mediated transformation β to α glycine [J].
Ferrari, ES ;
Davey, RJ ;
Cross, WI ;
Gillon, AL ;
Towler, CS .
CRYSTAL GROWTH & DESIGN, 2003, 3 (01) :53-60
[9]   RAMAN-SPECTROSCOPIC STUDY OF H2O AND D2O WATER SOLUTIONS OF GLYCINE [J].
FURIC, K ;
MOHACEK, V ;
BONIFACIC, M ;
STEFANIC, I .
JOURNAL OF MOLECULAR STRUCTURE, 1992, 267 :39-44
[10]   A reversible pressure-induced phase transition in β-glycine at 0.76 GPa [J].
Goryainov, SV ;
Kolesnik, EN ;
Boldyreva, E .
PHYSICA B-CONDENSED MATTER, 2005, 357 (3-4) :340-347
123