The processing and properties of (Zr, Hf)B2-SiC nanostructured composites

被引:40
作者
Wang, Hailong [1 ,2 ]
Lee, Sea-Hoon [2 ]
Feng, Lun [2 ]
机构
[1] Zhengzhou Univ, Sch Mat Sci & Engn, Zhengzhou 450001, Peoples R China
[2] Korea Inst Mat Sci, Div Powder Ceram Res, Chang Won 641831, Gyeongnam, South Korea
关键词
Spark plasma sintering; Mechanical properties; Borides; Nanocomposite; HIGH-TEMPERATURE CERAMICS; MECHANICAL-PROPERTIES; FRACTURE-TOUGHNESS; HFB2-SIC CERAMICS; DIBORIDE POWDERS; SIC PARTICLE; MICROSTRUCTURE; DENSIFICATION; ZRB2; NANOCOMPOSITE;
D O I
10.1016/j.jeurceramsoc.2014.05.020
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
(Zr, Hf)B-2-SiC nanostructured composites were fabricated by high energy ball milling and reactive spark plasma sintering (RSPS) of HfB2, ZrSi2, B4C and C. Highly dense composites with homogeneously intermixed ultra-fine (Zr, Hf)B-2 and SiC grains (100-300 nm) were obtained after RSPS at 1600 degrees C for 10 min. The densification was promoted by high energy ball milling and ZrSi2 additive. The additives were almost completely transformed into ZrB2 and SiC during densification. The improvement of flexural strength and fracture toughness (641 MPa and 5.36 MPa m(1/2), respectively) was achieved. The relationships between the ultra-fine microstructure and mechanical properties were discussed. (C) 2014 Elsevier Ltd. All rights reserved.
引用
收藏
页码:4105 / 4109
页数:5
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