Pesticides by solid-phase microextraction. Results of a round robin test

被引：51

作者：

Gorecki, T

Mindrup, R

Pawliszyn, J

机构：

[1] UNIV WATERLOO,DEPT CHEM,WATERLOO,ON N2L 3G1,CANADA

[2] SUPELCO INC,BELLEFONTE,PA 16823

来源：

ANALYST | 1996年 / 121卷 / 10期

关键词：

solid-phase microextraction; pesticide analysis; round robin test;

D O I：

10.1039/an9962101381

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

The applicability of solid-phase microextraction (SPME) for the analysis of semi-volatile compounds in water was verified by an interlaboratory study on pesticide analysis by SPME, Eleven laboratories in Europe and North America took part in the test. No previous experience with SPME was required, The test sample contained 12 pesticides representing all main groups (organochlorine, organonitrogen and organophosphate) at low ppb levels, The results of the test proved that SPME is an accurate and fast method of sample preparation and analysis, It can be an excellent alternative to currently used methods.

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收藏

页码：1381 / 1386

页数：6

相关论文

共 22 条

[1]

ARTHUR CL, 1992, HRC-J HIGH RES CHROM, V15, P741

[2] ANALYSIS OF SUBSTITUTED BENZENE COMPOUNDS IN GROUNDWATER USING SOLID-PHASE MICROEXTRACTION [J].

ARTHUR, CL ;

KILLAM, LM ;

MOTLAGH, S ;

LIM, M ;

POTTER, DW ;

PAWLISZYN, J .

ENVIRONMENTAL SCIENCE & TECHNOLOGY, 1992, 26 (05) :979-983

[3] SOLID-PHASE MICROEXTRACTION OF NITROGEN-CONTAINING HERBICIDES [J].

BOYDBOLAND, AA ;

PAWLISZYN, JB .

JOURNAL OF CHROMATOGRAPHY A, 1995, 704 (01) :163-172

[4] OPTIMIZATION OF SOLID-PHASE MICROEXTRACTION CONDITIONS FOR DETERMINATION OF PHENOLS [J].

BUCHHOLZ, KD ;

PAWLISZYN, J .

ANALYTICAL CHEMISTRY, 1994, 66 (01) :160-167

[5] DETERMINATION OF PHENOLS BY SOLID-PHASE MICROEXTRACTION AND GAS-CHROMATOGRAPHIC ANALYSIS [J].

BUCHHOLZ, KD ;

PAWLISZYN, J .

ENVIRONMENTAL SCIENCE & TECHNOLOGY, 1993, 27 (13) :2844-2848

[6] DETERMINATION OF VOLATILE CHLORINATED HYDROCARBONS IN AIR AND WATER WITH SOLID-PHASE MICROEXTRACTION [J].

CHAI, M ;

ARTHUR, CL ;

PAWLISZYN, J ;

BELARDI, RP ;

PRATT, KF .

ANALYST, 1993, 118 (12) :1501-1505

[7] DETERMINATION OF ORGANOPHOSPHORUS, TRIAZINE AND 2,6-DINITROANILINE PESTICIDES IN AQUEOUS SAMPLES VIA SOLID-PHASE MICROEXTRACTION (SPME) AND GAS-CHROMATOGRAPHY WITH NITROGEN-PHOSPHORUS DETECTION [J].

EISERT, R ;

LEVSEN, K .

FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY, 1995, 351 (06) :555-562

[8] ELEMENT-SELECTIVE DETECTION OF PESTICIDES BY GAS-CHROMATOGRAPHY ATOMIC-EMISSION DETECTION AND SOLID-PHASE MICROEXTRACTION [J].

EISERT, R ;

LEVSEN, K ;

WUNSCH, G .

JOURNAL OF CHROMATOGRAPHY A, 1994, 683 (01) :175-183

[9] BASICS OF INTERLABORATORY STUDIES - THE TRENDS IN THE NEW ISO-5725 STANDARD EDITION [J].

FEINBERG, M .

TRAC-TRENDS IN ANALYTICAL CHEMISTRY, 1995, 14 (09) :450-457

[10] Solid-phase microextraction of the herbicide metolachlor in runoff and tile-drainage water samples [J].

Graham, KN ;

Sarna, LP ;

Webster, GRB ;

Gaynor, JD ;

Ng, HYF .

JOURNAL OF CHROMATOGRAPHY A, 1996, 725 (01) :129-136