Optimization of rheological properties of photopolymerizable alumina suspensions for ceramic microstereolithography

被引:81
作者
Goswami, Ankur [1 ,2 ]
Ankit, K. [3 ]
Balashanmugam, N. [3 ]
Umarji, Arun M. [1 ]
Madras, Giridhar [2 ]
机构
[1] Indian Inst Sci, Mat Res Ctr, Bangalore 560012, Karnataka, India
[2] Indian Inst Sci, Ctr Nano Sci & Engn, Bangalore 560012, Karnataka, India
[3] Cent Mfg Technol Inst, Bangalore 560022, Karnataka, India
关键词
Microstereolithography; Alumina; Rheology; Ceramic processing; Fractal analysis; VISCOSITY; STEREOLITHOGRAPHY; DISPERSION;
D O I
10.1016/j.ceramint.2013.09.059
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Microstereolithography (MSL) is a rapid prototyping technique to fabricate complex three-dimensional (3D) structure in the microdomain involving different materials such as polymers and ceramics. The present effort is to fabricate microdimensional ceramics by the MSL system from a non-aqueous colloidal slurry of alumina. This slurry predominantly consists of two phases i.e. sub-micrometer solid alumina particles and non-aqueous reactive difunctional and trifunctional acrylates with inert diluent. The first part of the work involves the study of the stability and viscosity of the slurry using different concentrations of trioctyl phosphine oxide (TOPO) as a dispersant. Based on the optimization, the highest achievable solid loadings of alumina has been determined for this particular colloidal suspension. The second part of the study highlights the fabrication of several micro-dimensional alumina structures by the MSL system. (C) 2013 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
引用
收藏
页码:3655 / 3665
页数:11
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