Insights into nanocube-like morphological transformation of P25 by microwave-assisted hydrothermal method

被引:5
作者
Anel Perales-Martinez, I. [1 ]
Rodriguez-Gonzalez, Vicente [1 ]
Lee, Soo-Wohn [2 ]
机构
[1] IPICYT Inst Potosino Invest Cient & Tecnol, Div Mat Avanzados, San Luis Potosi 78216, SLP, Mexico
[2] Sun Moon Univ, Dept Environm Engn, Asan, South Korea
基金
新加坡国家研究基金会;
关键词
Square-shaped TiO2; HF capping agent; Nanocube-like TiO2; Microwave-assisted hydrothermal method; ANATASE TIO2 NANOSHEETS; NANOCRYSTALS; NANOSPHERES; STABILITY; GROWTH;
D O I
10.1016/j.matlet.2014.02.068
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Nanosized cuboid-like TiO2 with anatase-rutile structure was synthesized by using a microwave-assisted hydrothermal method. Silver nanoparticles, which were photoreduced on TiO2 P25 (STiO2), or TiO2 P25 was used as the precursor and HF was the source of F- ions, which played the role of capping agents. The synthesis was performed at pH 2 and 190 degrees C for 5 h. Fluorine species (HF) are important as stabilizing and shape-controlling agents which lead to the formation of TiO2 square-shaped plate nanoparticles. (C) 2014 Elsevier B.V. All rights reserved.
引用
收藏
页码:10 / 13
页数:4
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