One-pot synthesis of new-phase AgInSe2 nanorods

被引：125
作者：
ng, Me T. Ng
Boothroyd, Chris B.
Vittal, Jagadese J.
机构：
[1] Natl Univ Singapore, Dept Chem, Singapore 117543, Singapore
[2] Inst Mat Sci & Engn, Singapore 117602, Singapore
来源：
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY | 2006年 / 128卷 / 22期
关键词：
D O I：
10.1021/ja060543u
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
AgInSe2 nanorods with a previously unknown orthorhombic phase isostructural to AgInS2 have been prepared by the thermolysis of [(PPh3)2AgIn(SeC{O}Ph)4] in a mixture of oleylamine (OA) and dodecanethiol (DT) at 185 °C. A systematic study indicates that the ratio of surfactants is crucial for obtaining both monodispersed nanorods and the new orthorhombic phase AgInSe2. The AgInSe2 nanorods have been characterized by TEM, XRPD, EDX, and XPS. Copyright © 2006 American Chemical Society.
引用
收藏
页码：7118 / 7119
页数：2
相关论文
共 27 条
  • [11] Controlled synthesis of multi-armed CdS nanorod architectures using monosurfactant system
    Jun, YW
    Lee, SM
    Kang, NJ
    Cheon, J
    [J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2001, 123 (21) : 5150 - 5151
  • [12] KAZMERSKI LI, 1977, PHYS C SER, V35, P217
  • [13] Ligand-controlling synthesis and ordered assembly of ZnS nanorods and nanodots
    Li, YC
    Li, XH
    Yang, CH
    Li, YF
    [J]. JOURNAL OF PHYSICAL CHEMISTRY B, 2004, 108 (41) : 16002 - 16011
  • [14] Synthesis, structural characterization, photoluminescence and thermal properties of [(Ph3P)2Cu(μ-SeC{O}R)2Cu(PPh3)]
    Lu, Z
    Huang, W
    Vittal, JJ
    [J]. NEW JOURNAL OF CHEMISTRY, 2002, 26 (09) : 1122 - 1129
  • [15] Controlled growth of tetrapod-branched inorganic nanocrystals
    Manna, L
    Milliron, DJ
    Meisel, A
    Scher, EC
    Alivisatos, AP
    [J]. NATURE MATERIALS, 2003, 2 (06) : 382 - 385
  • [16] Shape and size control of Ag2Se nanocrystals from a single precursor [(Ph3P)3Ag2(SeC{O}Ph)2]
    Ng, MT
    Boothroyd, C
    Vittal, JJ
    [J]. CHEMICAL COMMUNICATIONS, 2005, (30) : 3820 - 3822
  • [17] Shape control of CdSe nanocrystals
    Peng, XG
    Manna, L
    Yang, WD
    Wickham, J
    Scher, E
    Kadavanich, A
    Alivisatos, AP
    [J]. NATURE, 2000, 404 (6773) : 59 - 61
  • [18] Synthesis and characterization of a size series of extremely small thiol-stabilized CdSe nanocrystals
    Rogach, AL
    Kornowski, A
    Gao, MY
    Eychmüller, A
    Weller, H
    [J]. JOURNAL OF PHYSICAL CHEMISTRY B, 1999, 103 (16) : 3065 - 3069
  • [19] SOLAR-CELLS MADE BY CHALCOPYRITE MATERIALS
    ROMEO, N
    [J]. JAPANESE JOURNAL OF APPLIED PHYSICS, 1980, 19 (03) : 5 - 13
  • [20] EFFICIENT CULNSE2/CDS SOLAR CELLS
    SHAY, JL
    WAGNER, S
    KASPER, HM
    [J]. APPLIED PHYSICS LETTERS, 1975, 27 (02) : 89 - 90
123