Pore structure characterization and permeability prediction of coal samples based on SEM images

被引:81
作者
Song, Shuai-Bing [1 ,2 ,3 ]
Liu, Jiang-Feng [1 ,2 ,3 ]
Yang, Dian-Sen [4 ]
Ni, Hong-Yang [1 ,2 ]
Huang, Bing-Xiang [5 ]
Zhang, Kai [1 ,2 ]
Mao, Xian-Biao [1 ,2 ]
机构
[1] China Univ Min & Technol, State Key Lab GeoMech & Deep Underground Engn, Xuzhou 221116, Jiangsu, Peoples R China
[2] China Univ Min & Technol, Sch Mech & Civil Engn, Xuzhou 221116, Jiangsu, Peoples R China
[3] Southwest Petr Univ, State Key Lab Oil & Gas Reservoir Geol & Exploita, Chengdu 610500, Sichuan, Peoples R China
[4] Chinese Acad Sci, Inst Rock & Soil Mech, State Key Lab Geomech & Geotech Engn, Wuhan 430071, Hubei, Peoples R China
[5] China Univ Min & Technol, State Key Lab Coal Resources & Safe Min, Xuzhou 221116, Jiangsu, Peoples R China
关键词
Gas permeability; Pore size distribution; SEM images; Pore structure; MERCURY INTRUSION POROSIMETRY; REPRESENTATIVE VOLUME ELEMENT; MAGNETIC-RESONANCE NMR; SIZE DISTRIBUTIONS; GAS-PERMEABILITY; MORPHOLOGY; EVOLUTION; POROSITY; DENSITY; BASIN;
D O I
10.1016/j.jngse.2019.05.003
中图分类号
TE [石油、天然气工业]; TK [能源与动力工程];
学科分类号
0807 ; 0820 ;
摘要
The pore structure of coal reservoirs determines the reserves of coalbed methane, and the gas permeability determines the level of the production capacity. In this study, the SEM images of coal samples were analyzed by various means. First, the grayscale threshold of binarization of the coal sample image is determined by a suitable algorithm. Comparing several different algorithms, the porosity based on Yen algorithm is closer to the results of vacuum saturation method and nuclear magnetic resonance (NMR) (8.35% vs. 7.51% vs. 8.92%). Further, the pore size distribution (PSD) of the coal sample is obtained according to discrete and continuous algorithms. By comparing the SEM results with the NMR results, it is found that the calculation results based on the continuous algorithm (CPSD) are better than the discrete algorithm (DPSD) and closer to the NMR results. For the effect of scale, we found that the image resolution has a certain influence on the minimum pore size characterized, such as sample Cl: 0.29 mu m ( x 1000) vs 0.58um ( x 500). At high resolution, more micro-pores are observed. Further, we predict the permeability of coal samples based on SEM images. It is found that the calculation results based on the continuous algorithm and the Hagen-Poiseuille equation are closer to the measured values (e.g., 16.97 (DPSD) vs. 0.45(CPSD) vs. 0.59 mD (Lab), sample C2, magnification of x 1000). In general, this method can effectively evaluate the pore structure characteristics and permeability of coal samples.
引用
收藏
页码:160 / 171
页数:12
相关论文
共 48 条
[11]   Permeability-porosity transforms from small sandstone fragments [J].
Kameda, A ;
Dvorkin, J ;
Keehm, Y ;
Nur, A ;
Bosl, W .
GEOPHYSICS, 2006, 71 (01) :N11-N19
[12]   A NEW METHOD FOR GRAY-LEVEL PICTURE THRESHOLDING USING THE ENTROPY OF THE HISTOGRAM [J].
KAPUR, JN ;
SAHOO, PK ;
WONG, AKC .
COMPUTER VISION GRAPHICS AND IMAGE PROCESSING, 1985, 29 (03) :273-285
[13]   Swelling-induced volumetric strains internal to a stressed coal associated with CO2 sorption [J].
Karacan, C. Ozgen .
INTERNATIONAL JOURNAL OF COAL GEOLOGY, 2007, 72 (3-4) :209-220
[14]   Adsorption and gas transport in coal microstructure: investigation and evaluation by quantitative X-ray CT imaging [J].
Karacan, CO ;
Okandan, E .
FUEL, 2001, 80 (04) :509-520
[15]   Characterization of multi-scale microstructural features in Opalinus Clay [J].
Keller, Lukas M. ;
Schuetz, Philipp ;
Erni, Rolf ;
Rossell, Marta D. ;
Lucas, Falk ;
Gasser, Philippe ;
Holzer, Lorenz .
MICROPOROUS AND MESOPOROUS MATERIALS, 2013, 170 :83-94
[16]   Investigation of pore size distributions of coals with different structures by nuclear magnetic resonance (NMR) and mercury intrusion porosimetry (MIP) [J].
Li, Xiangchen ;
Kang, Yili ;
Haghighi, Manouchehr .
MEASUREMENT, 2018, 116 :122-128
[17]   Research on water retention and microstructure characteristics of compacted GMZ bentonite under free swelling conditions [J].
Liu, Jiang-Feng ;
Ni, Hong-Yang ;
Chen, Yong-Gui ;
Wu, Yu ;
Song, Shuai-Bing ;
Cao, Xu-Lou ;
Bao, Wen-Bo ;
Pu, Hai ;
Mao, Xian-Biao .
ENVIRONMENTAL EARTH SCIENCES, 2018, 77 (16)
[18]   Investigation into water retention and gas permeability of Opalinus clay [J].
Liu, Jiang-feng ;
Wu, Yu ;
Cai, Cheng-Zheng ;
Ni, Hong-yang ;
Cao, Xu-lou ;
Pu, Hai ;
Song, Shuai-bing ;
Pu, Sheng-yan ;
Skoczylas, Frederic .
ENVIRONMENTAL EARTH SCIENCES, 2018, 77 (05)
[19]   Gas permeability of a compacted bentonite-sand mixture: coupled effects of water content, dry density, and confining pressure [J].
Liu, Jiang-Feng ;
Skoczylas, Frederic ;
Talandier, Jean .
CANADIAN GEOTECHNICAL JOURNAL, 2015, 52 (08) :1159-1167
[20]   Experimental research on water retention and gas permeability of compacted bentonite/sand mixtures [J].
Liu, Jiang-Feng ;
Skoczylas, Frederic ;
Liu, Jian .
SOILS AND FOUNDATIONS, 2014, 54 (05) :1027-1038