Frequent Pitfalls in the Characterization of Electrodes Designed for Electrochemical Energy Conversion and Storage

被引:37
作者
Zeradjanin, Aleksandar R. [1 ,2 ]
机构
[1] Forschungszentrum Julich, Helmholtz Inst Erlangen Nurnberg Renewable Energy, Egerlandstr 3, D-91058 Erlangen, Germany
[2] Max Planck Inst Eisenforsch GmbH, Dept Interface Chem & Surface Engn, Max Planck Str 1, D-40237 Dusseldorf, Germany
关键词
electrocatalysis; hydrogen; oxygen; rotating disk electrode; scanning electrochemical microscopy; OXYGEN REDUCTION REACTION; INTERRELATE INNER; CATALYST; ELECTROCATALYSIS; PERFORMANCE; IMPURITIES; EVOLUTION; SURFACE; MEDIA; AREAS;
D O I
10.1002/cssc.201702287
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Focus on the importance of energy conversion and storage boosted research interest in various electrocatalytic materials. Characterization of solid-liquid interfaces during faradaic and non-faradaic processes is routinely conducted in many laboratories worldwide on a daily basis. This can be deemed as a very positive tendency. However, careful insight into modern literature suggests frequent misuse of electroanalytical tools. This can have very negative implications and postpone overall development of electrocatalytic materials with the desired properties. This work points out some of the frequent pitfalls in electrochemical characterization, suggests potential solutions, and above all encourages comprehensive analysis and in-depth thinking about electrochemical phenomena.
引用
收藏
页码:1278 / 1284
页数:7
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