Determination of Bisphenol A in Water Using a Packed Needle Extraction Device

被引：22

作者：

Ogawa, Mitsuhiro ^{[1
]}

Saito, Yoshihiro ^{[1
]}

Shirai, Shingoro ^{[1
]}

Kiso, Yoshiaki ^{[2
]}

Jinno, Kiyokatsu ^{[1
]}

机构：

[1] Toyohashi Univ Technol, Sch Mat Sci, Toyohashi, Aichi 4418580, Japan

[2] Toyohashi Univ Technol, Dept Ecol Engn, Toyohashi, Aichi 4418580, Japan

来源：

CHROMATOGRAPHIA | 2009年 / 69卷 / 7-8期

基金：

日本学术振兴会;

关键词：

Gas chromatography; Fiber-packed needle; Bisphenol A; Derivatization; Water samples; POLYCYCLIC AROMATIC-HYDROCARBONS; SOLID-PHASE EXTRACTION; ENVIRONMENTAL-SAMPLES; MICROEXTRACTION; DESIGN; PAHS;

D O I：

10.1365/s10337-008-0928-4

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

A fiber-packed needle extraction device was used as a novel method for the extraction of bisphenol A from water samples. A bundle of filaments having a coating of polydimethylsiloxane was packed longitudinally into the needle. Good extraction efficiency was obtained even for an extraction time of 10 min, when the water sample was pumped through the needle with a syringe pump. The needle could be used repeatedly. The preparation procedure, included a derivatization process. Under optimum conditions, use of the fiber-packed needle showed a higher extraction efficiency than conventional sample preparation methods such as liquid-liquid extraction and solid-phase extraction.

引用

页码：685 / 690

页数：6

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