Synthesis and Crystal Structure of Aromatic Hydrazone Compounds Containing Pyrazole

被引:2
作者
Ren, Tiegang [1 ]
Liu, Shuyun [2 ]
Li, Yongzhe [1 ]
Li, Guihui [3 ]
Wang, Jie [1 ]
机构
[1] Henan Univ, Fine Chem & Engn Res Inst, Coll Chem & Chem Engn, Kaifeng 475004, Peoples R China
[2] Hunan City Univ, Yiyang 413000, Peoples R China
[3] Henan Univ, Key Lab, Minist Educ Special Funct Mat, Kaifeng 475004, Peoples R China
关键词
Aromatic hydrazone; Pyrazole; Synthesis; Crystal structure; Characterization;
D O I
10.1007/s10870-014-0521-7
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
Two novel aromatic hydrazone compounds containing pyrazole group were synthesized with 1-phenylpyrazole-4-carbaldehyde and benzene hydrazine (or p-tolylhydrazine hydrochloride) as the starting materials. As-synthesized aromatic hydrazone compounds were characterized by means of H-1 NMR, FT-IR, Ms and single-crystal X-ray diffraction. Results shown that two aromatic hydrazone compounds crystallizes in the monoclinic system of space group P21/n for A and Pc for B respectively.
引用
收藏
页码:346 / 351
页数:6
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