Synthesis and Crystal Structure of Aromatic Hydrazone Compounds Containing Pyrazole

被引:2
作者
Ren, Tiegang [1 ]
Liu, Shuyun [2 ]
Li, Yongzhe [1 ]
Li, Guihui [3 ]
Wang, Jie [1 ]
机构
[1] Henan Univ, Fine Chem & Engn Res Inst, Coll Chem & Chem Engn, Kaifeng 475004, Peoples R China
[2] Hunan City Univ, Yiyang 413000, Peoples R China
[3] Henan Univ, Key Lab, Minist Educ Special Funct Mat, Kaifeng 475004, Peoples R China
关键词
Aromatic hydrazone; Pyrazole; Synthesis; Crystal structure; Characterization;
D O I
10.1007/s10870-014-0521-7
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
Two novel aromatic hydrazone compounds containing pyrazole group were synthesized with 1-phenylpyrazole-4-carbaldehyde and benzene hydrazine (or p-tolylhydrazine hydrochloride) as the starting materials. As-synthesized aromatic hydrazone compounds were characterized by means of H-1 NMR, FT-IR, Ms and single-crystal X-ray diffraction. Results shown that two aromatic hydrazone compounds crystallizes in the monoclinic system of space group P21/n for A and Pc for B respectively.
引用
收藏
页码:346 / 351
页数:6
相关论文
共 50 条
[31]   Synthesis and herbicidal activity of novel pyrazole aromatic ketone analogs as HPPD inhibitor [J].
Fu, Qing ;
Cai, Peng-Peng ;
Cheng, Long ;
Zhong, Liang-Kun ;
Tan, Cheng-Xia ;
Shen, Zhong-Hua ;
Han, Liang ;
Xu, Tian-Ming ;
Liu, Xing-Hai .
PEST MANAGEMENT SCIENCE, 2020, 76 (03) :868-879
[32]   Crystal structure of aromatic polysulfones containing biphenylene units [J].
Ahmad, Zulkifli B. .
APPLICATIONS OF ENGINEERING MATERIALS, PTS 1-4, 2011, 287-290 :1548-1552
[33]   Synthesis and crystal structure of fluorine-containing α-aminophosphonates [J].
Yang, S ;
Song, BA ;
Wu, YL ;
Jin, LH ;
Liu, G ;
Hiu, DY ;
Lu, P .
CHINESE JOURNAL OF ORGANIC CHEMISTRY, 2004, 24 (10) :1292-1295
[34]   Synthesis, crystal structure and bacteriostatic activities of compounds derived from PMBP and aminophenol [J].
Wang, JL ;
Zhang, SM ;
Zhang, X ;
Miao, FM .
ACTA CHIMICA SINICA, 2003, 61 (07) :1071-1076
[35]   Synthesis and Crystal Structure of 1,3-disubstituted-2-propyleno-1-one Containing Pyrazole Moiety [J].
Y.-L. Zhou ;
X.-L. Wu ;
Fang-Ming Liu .
Journal of Chemical Crystallography, 2011, 41 :449-452
[36]   SYNTHESIS, CRYSTAL STRUCTURES, AND ANTIBACTERIAL ACTIVITY OF A SERIES OF HYDRAZONE COMPOUNDS DERIVED FROM 4-METHYLBENZOHYDRAZIDE [J].
Lei, Yan ;
Li, Ting-Zhen ;
Fu, Chuan ;
Guan, Xiao-Lin ;
Tan, Yao .
JOURNAL OF THE CHILEAN CHEMICAL SOCIETY, 2015, 60 (02) :2961-2965
[37]   Synthesis and biological activity of acyl thiourea containing difluoromethyl pyrazole motif [J].
Min, Li-Jing ;
Zhai, Zhi-Wen ;
Shi, Yan-Xia ;
Han, Liang ;
Tan, Cheng-Xia ;
Weng, Jian-Quan ;
Li, Bao-Ju ;
Zhang, Yong-Gang ;
Liu, Xing-Hai .
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2020, 195 (01) :22-28
[38]   Synthesis and Crystal Structure of 1,3-disubstituted-2-propyleno-1-one Containing Pyrazole Moiety [J].
Zhou, Y-L ;
Wu, X-L ;
Liu, Fang-Ming .
JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 2011, 41 (04) :449-452
[39]   Synthesis and Crystal Structure of Lanthanum Nitrate with Methyl-2-pyridyl Ketone Benzoyl Hydrazone [J].
TAI Xishi YIN Xianhong LIU Debo and TAN Minyu College of Chemistry and Chemical Engineering Lanzhou University Lanzhou P R China Department of Chemistry Guangxi University for Nationalities Nanning P R China YU Kaibei Analysis and Measurement Center Chengdu Branch of Chinese Academy of Sciences Chengdu P R China .
Chemical Research in Chinese Universities, 2003, (04) :434-436
[40]   Synthesis and crystal structure of lanthanum nitrate with methyl-2-pyridyl ketone benzoyl hydrazone [J].
Tai, XS ;
Yin, XH ;
Liu, DB ;
Tan, MY ;
Yu, KB .
CHEMICAL RESEARCH IN CHINESE UNIVERSITIES, 2003, 19 (04) :434-436