Structural evolutions of mechanically alloyed and heat treated Ti50C50 and Ti33B67 powders

被引:11
作者
Tang, W. M. [1 ]
Zheng, Z. X. [1 ]
Wu, W. C. [1 ]
Lu, J. [1 ]
Liu, J. W. [1 ]
Wang, J. M. [1 ]
机构
[1] Hefei Univ Technol, Sch Mat Sci & Engn, Hefei 230009, Peoples R China
关键词
TiC; TiB2; mechanical alloying; structural evolution; heat treatment; reaction mechanism;
D O I
10.1016/j.matchemphys.2005.09.085
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The TiC and TiB2 powders were successfully synthesized by ball milling the Ti50C50 and Ti33B67 elemental powders, respectively. During ball milling the Ti50C50 powder, a solid solution of C in Ti, Ti(C), was first formed, followed by TiC. After milling for 80 h, the powder was composed of TiC with grain size of 6 nm and a small amount of Ti(C) which was finally completely transformed to TiC after heat treatment. During ball milling the Ti33B67 powder, a solid solution of B in Ti, Ti(B), was first formed followed by the formation of an amorphous structure which transformed into a hexagonal phase of TiB2 with grain size of about 10 nm. (c) 2005 Elsevier B.V. All rights reserved.
引用
收藏
页码:144 / 149
页数:6
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