Total assignment of 1H and 13C NMR spectra of three triterpene saponins from roots of Silene vulgaris (Moench) Garcke

被引：23

作者：

Bouguet-Bonnet, S

Rochd, M

Mutzenhardt, P

Henry, M

机构：

[1] Univ Henri Poincare Nancy 1, CNRS, FRE 2415, Lab Methodol RMN,Fac Sci, F-54506 Vandoeuvre Les Nancy, France

[2] Univ Moulay, Fac Sci, Dept Biol, Meknes, Morocco

[3] Univ Henri Poincare Nancy 1, Lab Bot & Mycol, Fac Pharm, F-54001 Nancy, France

来源：

MAGNETIC RESONANCE IN CHEMISTRY | 2002年 / 40卷 / 09期

关键词：

NMR; H-1; C-13; saponins; gypsogenin; 3-O-glucuronide; quillaic acid 3-O-glucuronide; 3-O-glycoside; Silene vulgaris; Caryophyllaceae;

D O I：

10.1002/mrc.1069

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The assignments of H-1 and C-13 NMR spectra for three new triterpene saponins from Silene vulgaris (gypsogenin 3-O-glucuronide, quillaic acid 3-O-glucuronide, and gypsogenin 3-O-glycoside) are reported. In addition to ID NMR methods, 2D NMR techniques (COSY, HSQC, HMBC, and HSQC-TOCSY) were used for the assignments. Copyright (C) 2002 John Wiley Sons, Ltd.

引用

页码：618 / 621

页数：4

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