Nanoparticles Ni and NiO: Synthesis, characterization and magnetic properties

被引:279
作者
Davar, Fatemeh [1 ]
Fereshteh, Zeinab [1 ]
Salavati-Niasari, Masoud [1 ,2 ]
机构
[1] Univ Kashan, Inst Nanosci & Nanotechnol, Kashan, Iran
[2] Univ Kashan, Fac Sci, Dept Chem, Kashan, Iran
关键词
Nanoparticles; Ni; Inorganic materials; Characterization methods; Chemical synthesis; NANOCOMPOSITE MATERIALS; THERMAL-DECOMPOSITION; NICKEL; COLLOIDS; COMPLEX;
D O I
10.1016/j.jallcom.2008.09.121
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
The present investigation reports, the novel synthesis of nanoparticles Ni and NiO using thermal decomposition and their physicochemical characterization. The nanoparticles Ni powder have been prepared using [bis(2-hydroxyacetophenato)nickel(II)] as precursor. Transmission electron microscopy (TEM) analysis was demonstrated nanoparticles Ni with an average diameter of about 14-22 nm. The products were characterized by X-ray diffraction (XRD),TEM, high-resolution transmission electron microscopy(HRTEM) and Fourier transform infrared (FT-IR) spectroscopy. The magnetic property of Ni and NiO was studied with vibrating sample magnetometer (VSM). (C) 2008 Elsevier B.V. All rights reserved.
引用
收藏
页码:797 / 801
页数:5
相关论文
共 36 条
  • [1] Aharoni A., 1996, INTRO THEORY FERROMA, P133
  • [2] Preparation of porous nickel electrodes for molten carbonate fuel cells by non-aqueous tape casting
    Antolini, E
    Ferretti, M
    Gemme, S
    [J]. JOURNAL OF MATERIALS SCIENCE, 1996, 31 (08) : 2187 - 2192
  • [3] Synthesis of iron oxide nanoparticles used as MRI contrast agents: A parametric study
    Babes, L
    Denizot, B
    Tanguy, G
    Le Jeune, JJ
    Jallet, P
    [J]. JOURNAL OF COLLOID AND INTERFACE SCIENCE, 1999, 212 (02) : 474 - 482
  • [4] Nanocomposite materials for optical applications
    Beecroft, LL
    Ober, CK
    [J]. CHEMISTRY OF MATERIALS, 1997, 9 (06) : 1302 - 1317
  • [5] Spectroelectrochemistry of nanostructured NiO
    Boschloo, G
    Hagfeldt, A
    [J]. JOURNAL OF PHYSICAL CHEMISTRY B, 2001, 105 (15): : 3039 - 3044
  • [6] Chemisorption on nickel nanoparticles of various shapes: Influence on magnetism
    Cordente, N
    Amiens, C
    Chaudret, B
    Respaud, M
    Senocq, F
    Casanove, MJ
    [J]. JOURNAL OF APPLIED PHYSICS, 2003, 94 (10) : 6358 - 6365
  • [7] Surface spectroscopic study of carbon monoxide adsorption on nanoscale nickel colloids prepared from a zerovalent organometallic precursor
    deCaro, D
    Bradley, JS
    [J]. LANGMUIR, 1997, 13 (12) : 3067 - 3069
  • [8] SUPPORTED METAL-CLUSTERS - SYNTHESIS, STRUCTURE, AND CATALYSIS
    GATES, BC
    [J]. CHEMICAL REVIEWS, 1995, 95 (03) : 511 - 522
  • [9] Structural and magnetic properties of hcp and fcc Ni nanoparticles
    Gong, J.
    Wang, L. L.
    Liu, Y.
    Yang, J. H.
    Zong, Z. G.
    [J]. JOURNAL OF ALLOYS AND COMPOUNDS, 2008, 457 (1-2) : 6 - 9
  • [10] Hafeli U., 1997, Scientific and Clinical Applications of Magnetic Carriers