CO2-supercritical extraction, hydrodistillation and steam distillation of essential oil of rosemary (Rosmarinus officinalis)

被引:123
作者
Conde-Hernandez, Lilia A. [1 ]
Espinosa-Victoria, Jose R. [1 ]
Trejo, Arturo [2 ]
Guerrero-Beltran, Jose A. [1 ]
机构
[1] Univ Americas Puebla, Dept Ingn Quim Alimentos & Ambiental, Cholula 72810, Mexico
[2] Inst Mexicano Petr, Lab Thermodynam Thermophys Res Area Solubil, Mexico City, DF, Mexico
关键词
Rosemary; Rosmarinus officinalis; Supercritical extraction; Hydrodistillation; Steam distillation; Antioxidant activity; SUPERCRITICAL-FLUID EXTRACTION; PERFORMANCE LIQUID-CHROMATOGRAPHY; CHEMICAL-COMPOSITION; CARBON-DIOXIDE; ANTIOXIDANT; L; FRACTIONATION;
D O I
10.1016/j.jfoodeng.2016.12.022
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
Essential oil of rosemary was obtained by supercritical CO2-extraction (SCE), hydrodistillation (HYDRO), and steam distillation (SD). Quantity of oil, antioxidant activity, and chemical composition (gas chromatography-mass spectrometry, GC -MS) of the essential oils were evaluated. For SCE, oil was obtained at two temperatures (40 and 50 degrees C) and two pressures (1034 and 17.24 MPa) using a rosemary particle size of 600 +/- 50 mu m. The yield was between 1.41 and 2.53 g essential oil (EO) 100 g(-1) of dry rosemary (% wow). The antioxidant activity values were in the range 29.67-37.55 mg equivalent of Trolox (ET) g(-1) of EO or 22.66-30.81 mg ascorbic acid (AA) g(-1) of EO. Yields of essential oil were between 0.35 and 2.35%. The antioxidant activity was found in the range 1.73-2.60 Mg ET g(-1) of EO or 1,50-2.20 mg AA g(-1) of EO. Camphor, eucalyptol, beta-caryophyllene, and borneol acetate were the main chemicals detected by GC -MS in EO. (C) 2017 Elsevier Ltd. All rights reserved.
引用
收藏
页码:81 / 86
页数:6
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