CO2-supercritical extraction, hydrodistillation and steam distillation of essential oil of rosemary (Rosmarinus officinalis)

被引：123
作者：
Conde-Hernandez, Lilia A. [1 ]
Espinosa-Victoria, Jose R. [1 ]
Trejo, Arturo [2 ]
Guerrero-Beltran, Jose A. [1 ]
机构：
[1] Univ Americas Puebla, Dept Ingn Quim Alimentos & Ambiental, Cholula 72810, Mexico
[2] Inst Mexicano Petr, Lab Thermodynam Thermophys Res Area Solubil, Mexico City, DF, Mexico
来源：
JOURNAL OF FOOD ENGINEERING | 2017年 / 200卷
关键词：
Rosemary; Rosmarinus officinalis; Supercritical extraction; Hydrodistillation; Steam distillation; Antioxidant activity; SUPERCRITICAL-FLUID EXTRACTION; PERFORMANCE LIQUID-CHROMATOGRAPHY; CHEMICAL-COMPOSITION; CARBON-DIOXIDE; ANTIOXIDANT; L; FRACTIONATION;
D O I：
10.1016/j.jfoodeng.2016.12.022
中图分类号：
TQ [化学工业];
学科分类号：
0817 ;
摘要：
Essential oil of rosemary was obtained by supercritical CO2-extraction (SCE), hydrodistillation (HYDRO), and steam distillation (SD). Quantity of oil, antioxidant activity, and chemical composition (gas chromatography-mass spectrometry, GC -MS) of the essential oils were evaluated. For SCE, oil was obtained at two temperatures (40 and 50 degrees C) and two pressures (1034 and 17.24 MPa) using a rosemary particle size of 600 +/- 50 mu m. The yield was between 1.41 and 2.53 g essential oil (EO) 100 g(-1) of dry rosemary (% wow). The antioxidant activity values were in the range 29.67-37.55 mg equivalent of Trolox (ET) g(-1) of EO or 22.66-30.81 mg ascorbic acid (AA) g(-1) of EO. Yields of essential oil were between 0.35 and 2.35%. The antioxidant activity was found in the range 1.73-2.60 Mg ET g(-1) of EO or 1,50-2.20 mg AA g(-1) of EO. Camphor, eucalyptol, beta-caryophyllene, and borneol acetate were the main chemicals detected by GC -MS in EO. (C) 2017 Elsevier Ltd. All rights reserved.
引用
收藏
页码：81 / 86
页数：6
相关论文
共 50 条
[31]   Antioxidant activity of rosemary (Rosmarinus officinalis L.) essential oil and its hepatoprotective potential [J].
Raskovic, Aleksandar ;
Milanovic, Isidora ;
Pavlovic, Nebojsa ;
Cebovic, Tatjana ;
Vukmirovic, Sasa ;
Mikov, Momir .
BMC COMPLEMENTARY AND ALTERNATIVE MEDICINE, 2014, 14
[32]   Hydrodistillation and Steam Distillation of Fennel Seeds Essential Oil: Parameter Optimization and Application of Cryomilling Pretreatment [J].
Marcac, Nina ;
Balbino, Sandra ;
Tonkovic, Petra ;
Medved, Ana Marija ;
Cegledi, Ena ;
Dragovic, Sanja ;
Dragovic-Uzelac, Verica ;
Repajic, Maja .
PROCESSES, 2023, 11 (08)
[33]   The influence of genetic variation on essential oil composition in Rosmarinus officinalis L., the common rosemary [J].
Tawfeeq, A. ;
Culham, A. ;
Davis, F. ;
Reeves, M. ;
Michael, N. .
PLANTA MEDICA, 2016, 82
[34]   A study on the extraction of essential oil of Persian black cumin using static supercritical CO2 extraction, and comparison with hydro-distillation extraction method [J].
Zarrinpashne, Saeed ;
Kandi, Soheila Gorji .
SEPARATION SCIENCE AND TECHNOLOGY, 2019, 54 (11) :1778-1786
[35]   The extraction of rosemary essential oil by microwave-assisted hydrodistillation method [J].
Dinh, P. N. ;
Thuy, L. M. T. ;
Quoc, T. P. .
5TH INTERNATIONAL CONFERENCE OF CHEMICAL ENGINEERING AND INDUSTRIAL BIOTECHNOLOGY (ICCEIB 2020), 2020, 991
[36]   Comparison of pennyroyal oils obtained by supercritical CO2 extraction and hydrodistillation [J].
Reis-Vasco, EMC ;
Coelho, JAP ;
Palavra, AMF .
FLAVOUR AND FRAGRANCE JOURNAL, 1999, 14 (03) :156-160
[37]   Simultaneous Hydrodistillation-Steam Distillation of Rosmarinus officinalis, Lavandula angustifolia and Citrus aurantium from Morocco, Major Terpenes: Impact on Biological Activities [J].
El Kharraf, Sara ;
Faleiro, Maria Leonor ;
Abdellah, Farah ;
El-Guendouz, Soukaina ;
El Hadrami, El Mestafa ;
Miguel, Maria Graca .
MOLECULES, 2021, 26 (18)
[38]   Deterpenation of rosemary (Rosmarinus officinalis var. typicus L.) leaf essential oil using a mathematical model of kinetic guided hydrodistillation [J].
Walid, Yeddes ;
Majdi, Hammami ;
Wissem, Aidi Wannes ;
Khammassi, Saber ;
Mahmoud, Gargouri ;
Manef, Abderrabba ;
Ksouri, Riadh ;
Tounsi, Moufida Saidani .
JOURNAL OF ESSENTIAL OIL RESEARCH, 2019, 31 (03) :235-246
[39]   Comparison Extraction Methods of Essential oils of Rosmarinus officinalis L. in Iran By Microwave Assisted Water Distillation; Water Distillation and Steam Distillation [J].
Jaimand, Kamkar ;
Rezaee, Mohammad Bagher ;
Homami, Saied .
JOURNAL OF MEDICINAL PLANTS AND BY-PRODUCTS-JMPB, 2018, 7 (01) :9-14
[40]   Supercritical fluid extraction from rosemary (Rosmarinus officinalis):: Kinetic data, extract's global yield, composition, and antioxidant activity [J].
Carvalho, RN ;
Moura, LS ;
Rosa, PTV ;
Meireles, MAA .
JOURNAL OF SUPERCRITICAL FLUIDS, 2005, 35 (03) :197-204
12345