Miniaturized solid-phase extraction techniques

被引:390
作者
Plotka-Wasylka, Justyna [1 ]
Szczepanska, Natalia [1 ]
de la Guardia, Miguel [2 ]
Namiesnik, Jacek [1 ]
机构
[1] Gdansk Univ Technol, Fac Chem, Dept Analyt Chem, PL-80233 Gdansk, Poland
[2] Univ Valencia, Dept Analyt Chem, E-46100 Valencia, Spain
关键词
Dispersive solid-phase extraction; Green analytical chemistry; Immunoaffinity solid-phase extraction; Magnetic solid-phase extraction; Microextraction in a packed syringe; Miniaturized solid-phase extraction; Molecularly-imprinted solid-phase extraction; Solid-phase extraction; Solid-phase microextraction; Stir-bar sorptive extraction; BAR SORPTIVE EXTRACTION; POLYCYCLIC AROMATIC-HYDROCARBONS; MOLECULARLY IMPRINTED POLYMER; PERFORMANCE LIQUID-CHROMATOGRAPHY; AGENT DEGRADATION-PRODUCTS; BIOLOGICAL SAMPLES PRIOR; WALLED CARBON NANOTUBES; MASS-SPECTROMETRY; MAGNETIC NANOPARTICLES; PACKED SORBENT;
D O I
10.1016/j.trac.2015.04.026
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
More than 80% of analysis time is spent on sample collection and sample preparation, so sample preparation is a critical part of the analytical process. Traditionally, liquid-liquid extraction was developed and employed to screen for general unknowns. However, solid-phase extraction (SPE) is becoming highly popular as an alternative, due to its simplicity and economy in terms of time and solvent. This review summarizes the current state of the art and the future prospects for green analytical chemistry with special emphasis on environment-friendly sample-preparation techniques based on the solid phase. We discuss in detail miniaturized SPE techniques, based on the most relevant, most representative and most recent scientific references. (C) 2015 Elsevier B.V. All rights reserved.
引用
收藏
页码:19 / 38
页数:20
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