Molecular iodine-catalyzed facile procedure for N-boc protection of amines

被引：173
|
作者：
Varala, Ravi [1 ]
Nuvula, Sreelatha [1 ]
Adapa, Srinivas R. [1 ]
机构：
[1] Indian Inst Chem Technol, Hyderabad 500007, Andhra Pradesh, India
来源：
JOURNAL OF ORGANIC CHEMISTRY | 2006年 / 71卷 / 21期
关键词：
CERIC AMMONIUM-NITRATE; TERT-BUTOXYCARBONYLATION; LANTHANIDE TRIFLATE; EFFICIENT SYNTHESIS; CARBONYL-COMPOUNDS; ORGANIC-SYNTHESIS; MICHAEL ADDITION; ARYL AMINES; ACID; DERIVATIVES;
D O I：
10.1021/jo0612473
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
An efficient and practical protocol for the protection of various structurally and electronically divergent aryl and aliphatic amines using (Boc)(2)O in the presence of a catalytic amount of molecular iodine (10 mol %) under solvent-free conditions at ambient temperature is presented.
引用
收藏
页码：8283 / 8286
页数：4
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