Monetite formed in mixed solvents of water and ethylene glycol and its transformation to hydroxyapatite

被引：112

作者：

Ma, Ming-Guo

Zhu, Ying-Jie ^{[1
]}

Chang, Jiang

机构：

[1] Chinese Acad Sci, Shanghai Inst Ceram, Biomat & Tissue Engn Res Ctr, State Key Lab High Performance Ceram & Superfine, Shanghai 200050, Peoples R China

[2] Chinese Acad Sci, Grad Sch, Beijing 100864, Peoples R China

来源：

JOURNAL OF PHYSICAL CHEMISTRY B | 2006年 / 110卷 / 29期

关键词：

D O I：

10.1021/jp061738r

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

Agglomerated nanorods of hydroxyapatite have been synthesized using monetite as a precursor in a NaOH solution. Monetite consisting of nanosheets has been successfully synthesized by a one-step microwave-assisted method using CaCl(2)(.)2.5H(2)O, NaH2PO4, and sodium dodecyl sulfate (SDS) in water/ethylene glycol (EG) mixed solvents. The effects of the molar ratio of water to EG and the reaction time on the products were investigated. The products were characterized by X-ray powder diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy ( TEM), and Fourier transform infrared spectrometry (FTIR).

引用

页码：14226 / 14230

页数：5

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