Oxygen-Sensing Properties of Electrospun CNTs/PVAc/TiO2 Composites

被引:15
作者
Frontera, P. [1 ]
Trocino, S. [1 ]
Donato, A. [1 ]
Antonucci, P. L. [1 ]
Lo Faro, M. [2 ]
Squadrito, G. [2 ]
Neri, G. [3 ]
机构
[1] Univ Mediterranea Reggio Calabria, Dept Civil Engn Energy Environm & Mat, I-89124 Reggio Di Calabria, Italy
[2] CNR ITAE Nicola Giordano, I-98126 Messina, Italy
[3] Univ Messina, Dept Elect Engn Chem & Ind Engn, I-98166 Messina, Italy
关键词
oxygen sensor; electrospinning; MWCNTS; TIO2; composite materials; THERMAL-DEGRADATION; TEMPERATURE; SENSOR; FILM; NANOFIBER; THICK;
D O I
10.1007/s13391-013-3079-1
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Multi-walled-carbon-nanotubes/polyvinylacetate/titanium oxide (MWCNTs/PVAc/TiO2) composite fibers with different MWCNT loadings were prepared using the electrospinning technique. The addition of cetyl trimethyl ammonium bromide (CTAB) as a surfactant agent to promote the dispersion of the MWCNTs was also evaluated. The morphological and microstructural properties of as-spun and annealed samples in air at 600 degrees C were examined using thermogravimetric analysis (TGA), Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM) and x-ray diffraction (XRD). The sensing characteristics of the synthesized TiO2-based nanostructures were evaluated for oxygen monitoring at moderate temperatures. The effects of the MWCNT loading, the addition of the surfactant and the composition of the TiO2 crystalline phases were investigated and discussed.
引用
收藏
页码:305 / 313
页数:9
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