Crystal Structure of E-methyl-2-(1,3-Dimethyl-2,6-Diphenylpiperidin-4-Ylidene) Hydrazinecarboxylate Compound

被引：0
|
作者：
Mohandas, T. [1 ]
Sakthivel, P. [2 ]
Udhayakumar, C. [3 ]
Prakasam, B. Arul [3 ]
Butcher, Ray J. [4 ]
机构：
[1] Shri Angalamman Coll Engn & Technol, Dept Phys, Tiruchirappalli 621105, India
[2] Urumu Dhanalakshmi Coll, Dept Phys, Tirchy 620019, India
[3] Annamalai Univ, Dept Chem, Chidambaram, India
[4] Howard Univ, Inorgan & Struct Chem, Washington, DC 20059 USA
来源：
RECENT TRENDS IN MATERIALS SCIENCE AND APPLICATIONS | 2017年 / 189卷
关键词：
D O I：
10.1007/978-3-319-44890-9_49
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title compound crystallizes with three molecules and this compound. The structure was solved by SHELXS and it was refined by SHELXL. This compound adopts triclinic crystal systems with the space group P-1. The two phenyl rings are attached with the centre piperidine ring on each side and the methyl 2-methylene hydrazinecarboxylate system is connected to top of the piperidine ring. In each molecule the piperidine ring exhibits the chair conformations with the corresponding puckering parameters. The final R indices of this structure is 0.061. The bond lengths, torsion angles are calculated and it was tabulated. The molecules are linked by N-H center dot center dot center dot O interactions and this interactions makes the graph set motif of R-4(4)(8). In this structure the C-H center dot center dot center dot O interactions are also found.
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收藏
页码：535 / 541
页数：7
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