Pulsed field gradients in NMR high resolution experiments

被引:0
作者
Espinoza, L [1 ]
Garbarino, JA [1 ]
Chamy, MC [1 ]
Piovano, M [1 ]
机构
[1] Univ Tecn Federico Santa Maria, Dept Quim, Lab Prod Nat, Lab RMN V Reg, Valparaiso, Chile
关键词
D O I
10.4067/S0717-97072004000200016
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
High-resolution NMR spectra of selective 1D, 2D homonuclear and 2D heteronuclear experiments were registered of the mixtures of the natural products 3-4 and the methyl esters (5-6) and acetyl derivates (7-8) of the natural product 1-2, using Pulsed Field Gradients (PFGs) technique. Thus. it was possible to obtain high-resolution spectra, smaller time of acquisition and larger structural information.
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页码:189 / 195
页数:7
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