Enantiomeric separation of four chiral compounds using immobilized cellulose 3, 5-dimethylphenylcarbamate as chiral stationary phase

被引：0
作者：
Ming, Yong Fei
Zhao, Liang
Zhang, Hong Li
Shi, Yan Ping
Li, Yong Min [1 ]
Chen, Li Ren
机构：
[1] Chinese Acad Sci, Lanzhou Inst Chem Phys, Key Lab Nat Med Gansu Prov, Lanzhou 730000, Peoples R China
[2] Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China
来源：
CHINESE CHEMICAL LETTERS | 2006年 / 17卷 / 09期
关键词：
HPLC; immobilized; enantiomeric separation;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A new chiral stationary phase of 3, 5-dimethylphenylcarbamates of cellulose, chemically bonded to 3-aminopropylsilica gel at the 6-positions of the glucose units, was prepared. The solvent versatility of the CSP was investigated for the enantioselective separation of four pairs of enantiomers using THF and chloroform as non-standard mobile phase eluent in HPLC. The influence of temperature on the resolution was investigated.
引用
收藏
页码：1213 / 1216
页数：4
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