Enantiomeric separation of four chiral compounds using immobilized cellulose 3, 5-dimethylphenylcarbamate as chiral stationary phase

被引：0

作者：

Ming, Yong Fei

Zhao, Liang

Zhang, Hong Li

Shi, Yan Ping

Li, Yong Min ^{[1
]}

Chen, Li Ren

机构：

[1] Chinese Acad Sci, Lanzhou Inst Chem Phys, Key Lab Nat Med Gansu Prov, Lanzhou 730000, Peoples R China

[2] Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China

来源：

CHINESE CHEMICAL LETTERS | 2006年 / 17卷 / 09期

关键词：

HPLC; immobilized; enantiomeric separation;

D O I：

暂无

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

A new chiral stationary phase of 3, 5-dimethylphenylcarbamates of cellulose, chemically bonded to 3-aminopropylsilica gel at the 6-positions of the glucose units, was prepared. The solvent versatility of the CSP was investigated for the enantioselective separation of four pairs of enantiomers using THF and chloroform as non-standard mobile phase eluent in HPLC. The influence of temperature on the resolution was investigated.

引用

页码：1213 / 1216

页数：4

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