Synthesis and X-ray structure of a novel N′-ferrocenylmethyl-N′-phenylbenzohydrazide

被引：0
|
作者：
Terki, B. [1 ]
Lanez, T. [1 ]
Belaidi, S. [1 ]
Gornitzka, H. [1 ]
Ourari, A. [1 ]
机构：
[1] Univ Ouargla, VPRS Lab, Ouargla 30000, Algeria
来源：
ASIAN JOURNAL OF CHEMISTRY | 2006年 / 18卷 / 03期
关键词：
ferrocene; N '-ferrocenylmethyl-N '-phenylbenzohydrazide; X-ray crystal structure; molecular modelling; cyclic voltammetry;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Reaction of ferrocenylmethyltrimethylammonium iodide with N'-phenylbenzohydrazide afforded a novel stable N'-feffocenylmethyl-N'-phenylbenzohydrazide which was characterized by H-1 and C-13 NMR, mass spectroscopy and X-ray crystallography. The product crystallizes in the orthorhombic space group Pbca. The structure analysis confirms the optimized geometry obtained by molecular modelling calculations. The electrochemical behaviour of the N'-ferrocenylmethyl-N'-phenylbenzohydrazide derivative has been studied by cyclic voltammetry.
引用
收藏
页码：2074 / 2080
页数：7
相关论文
共 50 条
  • [1] ELECTROCHEMICAL STUDIES OF N '-FERROCENYLMETHYL-N '-PHENYLBENZOHYDRAZIDE AT GLASSY CARBON ELECTRODE IN DIFFERENT MEDIUM
    Khelef, A.
    Neghmouche, N. S.
    Lanez, T.
    JOURNAL OF FUNDAMENTAL AND APPLIED SCIENCES, 2011, 3 (02) : 200 - 209
  • [2] N'-Ferrocenylmethyl-N'-phenylbenzohydrazide as a potential DNA binding compound: a combined experimental and computational study
    Hanane, Mouada
    Lanez, Touhami
    Zafar, Imran
    Afghan, Muhammad Sher
    Zegheb, Nadjiba
    JOURNAL OF COORDINATION CHEMISTRY, 2023, 76 (16-24) : 1984 - 1998
  • [3] N,N-bis(quinonyl)amines;: synthesis and X-ray structure
    Bittner, S
    Meenakshi, C
    Temtsin, G
    TETRAHEDRON, 2001, 57 (34) : 7423 - 7429
  • [4] Synthesis, structure, electrochemical and antimicrobial properties of N,N′-bis(ferrocenylmethyl)imidazolinium salts
    Ozbek, Hulya Avci
    Aktas, Pelin Sozen
    Daran, Jean-Claude
    Oskay, Mustafa
    Demirhan, Funda
    Cetinkaya, Bekir
    INORGANICA CHIMICA ACTA, 2014, 423 : 435 - 442
  • [5] Synthesis and characterization of novel derivatives of N-(ferrocenesulfonyl)carbamic acid.: X-ray structure determination of ferrocenesulfonamide and N-(ferrocenesulfonyl)-N′-butylurea
    Besenyei, G
    Parkanyi, L
    Nemeth, S
    Simandi, LI
    JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1998, 563 (1-2) : 81 - 86
  • [6] ROS scavenging, DNA binding and NADPH oxidase inhibition potential of N′-Ferrocenylmethyl-N′- phenylpropionohydrazide using cyclic voltammetry and molecular docking
    Mouada, Hanane
    Lanez, Touhami
    Zafar, Imran
    JOURNAL OF ORGANOMETALLIC CHEMISTRY, 2024, 1007
  • [7] Ferrocene derivatives (I).: Synthesis and X-ray structure determination of N-o-methylphenylferrocenesulfonamide
    Li, M
    Bai, YJ
    Lu, J
    Yang, BQ
    Zhu, KK
    Ma, HR
    JOURNAL OF ORGANOMETALLIC CHEMISTRY, 2001, 637 : 738 - 741
  • [8] Synthesis, structural characterisation and biological activity of novel N-(ferrocenylmethyl)benzene-carboxamide derivatives
    Kelly, Paula N.
    Pretre, Adeline
    Devoy, Siobhan
    O'Rielly, Isobel
    Devery, Rosaleen
    Goel, Alok
    Gallagher, John F.
    Lough, Alan J.
    Kenny, Peter T. M.
    JOURNAL OF ORGANOMETALLIC CHEMISTRY, 2007, 692 (06) : 1327 - 1331
  • [9] Synthesis and x-ray crystal structure of the chiral ligand (S,R)-N,N-diethyl-N′-(2-(N",N"-dimethyl-1-aminoethyl))ferrocenoylthiourea
    Beyer, L
    Richter, R
    Seidelmann, O
    JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1998, 561 (1-2) : 199 - 201
  • [10] Synthesis and X-ray crystal structure of two novel ester ferrocenophanes
    Department of Chemistry, Northwest University, Xi'an, Shaanxi 710069, China
    Z. Naturforsch. Sect. B J. Chem. Sci., 2007, 4 (605-609): : 605 - 609
12345