Synthesis and Crystal Structure of a New Mn(II) Coordination Polymer With a Self-Catenane Rob Topology

被引：1

作者：

Zhang, Xiuling ^{[1
]}

Qiu, Yu'e ^{[1
]}

Jin, Feng ^{[2
]}

Guo, Feng ^{[1
]}

机构：

[1] Dezhou Univ, Key Lab Coordinat Chem & Funct Mat Univ Shandong, Dezhou 253023, Shandong, Peoples R China

[2] Dezhou Univ, Dept Phys, Dezhou 253023, Shandong, Peoples R China

来源：

SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY | 2014年 / 44卷 / 09期

关键词：

crystal structure; coordination polymer; Mn(II); METAL-ORGANIC FRAMEWORKS; HYDROTHERMAL SYNTHESIS; ACID; LIGANDS;

D O I：

10.1080/15533174.2013.799209

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A new coordination polymer, {[Mn(bpdc)(bibp)]center dot H2O}(n) (1) (H(2)bpdc = biphenyl- 2,4 '-dicarboxylate and bibp = 4,4 '-bis(imidazol-1-yl)biphenyl), has been prepared by hydrothermal synthesis and characterized by single-crystal X-ray diffraction, IR and EA. Complex, {[Mn(bpdc)(bibp)]center dot H2O}(n) (1), is monoclinic, space group C2/c with a = 34.453 (5) angstrom, b = 10.028 (5) angstrom, c = 19.310 (5)angstrom, beta = 122.760 (5)degrees, V = 5610 (3) angstrom(3), Z = 8, M-r = 599.49, D-c = 1.419g/cm(3), F(000) = 2472 and mu = 0.52mm(-1). The final refinement gave R = 0.0404 and wR = 0.1029 for reflections with I > 2 sigma(I). X-ray diffraction analysis reveals that the title complex {[Mn(bpdc)(bibp)]center dot H2O}(n)(1) displays a self- catenane rob topological network.

引用

页码：1278 / 1281

页数：4

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