Preparation of nanocrystalline ceria particles by sonochemical and microwave assisted heating methods

被引：185

作者：

Wang, H

Zhu, JJ ^{[1
]}

Zhu, JM

Liao, XH

Xu, S

Ding, T

Chen, HY

机构：

[1] Nanjing Univ, Lab Mesoscop Mat Sci, Nanjing 210093, Peoples R China

[2] Nanjing Univ, State Key Lab Coordinat Chem, Dept Chem, Nanjing 210093, Peoples R China

[3] Nanjing Univ, Solid State Microstruct Lab, Nanjing 210093, Peoples R China

[4] Huanggang Normal Univ, Hubei 438000, Peoples R China

来源：

PHYSICAL CHEMISTRY CHEMICAL PHYSICS | 2002年 / 4卷 / 15期

关键词：

D O I：

10.1039/b201394k

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

Nanocrystalline ceria (CeO2) particles have been successfully prepared via sonochemical and microwave assisted heating routes from aqueous solutions containing (NH4)(2)Ce(NO3)(6), hexamethylenetetramine and poly ( ethylene glycol)-19000 ( PEG). The products were characterized by techniques such as powder X-ray diffraction, transmission electron microscopy, high-resolution transmission electron microscopy, selected area electron diffraction, Brunauer-Emmett-Teller nitrogen adsorption and UV-Visible absorption spectroscopy. Analysis of the results showed that the products had uniform shape, narrow size distribution and displayed conspicuous quantum size effects.

引用

页码：3794 / 3799

页数：6