Sensitive colorimetric detection of ascorbic acid based on seed mediated growth of sodium alginate reduced/stabilized gold nanoparticles

被引:33
作者
Jayeoye, Titilope John [1 ,2 ,3 ,4 ]
Sirimahachai, Uraiwan [1 ,2 ]
Rujiralai, Thitima [1 ,2 ,3 ]
机构
[1] Prince Songkla Univ, Fac Sci, Ctr Excellence Innovat Chem, Hat Yai 90112, Songkhla, Thailand
[2] Prince Songkla Univ, Fac Sci, Div Phys Sci, Hat Yai 90112, Songkhla, Thailand
[3] Prince Songkla Univ, Fac Sci & Technol, Analyt Chem & Environm Res Unit, Pattani 94000, Thailand
[4] Alex Ekwueme Fed Univ, Dept Chem Biochem Mol Biol, Abakaliki, Ebonyi State, Nigeria
关键词
Alginate; Nanoparticles; Ascorbic acid; Colorimetry; Vitamin C; Fruit juice; SILVER NANOPARTICLES; GREEN SYNTHESIS; CROSS-LINKING; ANTIBACTERIAL; DOPAMINE; SENSOR;
D O I
10.1016/j.carbpol.2020.117376
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
A sensitive detection strategy for ascorbic acid (AA), using sodium alginate reduced/stabilized gold nanoparticles (SA-AuNPs) as the optical probe, is reported. The SA-AuNPs were prepared by mixing gold salt and SA under stirring for 2 h at room temperature, without any further steps. The mixture was aged at 4 degrees C overnight, after which a faint-purple colloidal solution of SA-AuNPs was obtained. Characterization shows that the synthesis is incapable of reducing all Au3+ to Au degrees, but rather to mixture of Au degrees/Au+. The addition of AA to the SA-AuNPs probe reduced completely all Au+ to new AuNPs which were deposited on the pre-formed SA-AuNPs seed, leading to size increment and absorption spectra enhancement. The assay exhibited a good linearity between 12.5 and 150.0 mu M AA and low limit of quantification of 11.2 mu M. It was further used for AA quantitation in vitamin C injection and fruit juice with satisfactory accuracy and precision.
引用
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页数:9
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