Studies on Y2O3:Eu phosphor with different particle size prepared by wet chemical method

被引:26
作者
Muresan, Laura [1 ]
Popovici, Elisabeth Jeanne [1 ]
Imre-Lucaci, Florica [1 ]
Grecu, Rodica [1 ]
Indrea, Emil [2 ]
机构
[1] Raluca Ripon Inst Res Chem, Cluj Napoca 400294, Romania
[2] Natl Inst R&D Isotop & Mol Technol, Cluj Napoca 400295, Romania
关键词
Phosphors; Chemical synthesis; Scanning electron microscopy; X-ray diffraction; CRYSTALLITE SIZE; YTTRIUM; INTENSITY;
D O I
10.1016/j.jallcom.2008.08.087
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Europium activated yttrium oxide phosphors were prepared by reagent simultaneous addition technique, using oxalic acid as precipitating reagent. The aim of the paper is to establish the flux influence and thermal regime on photoluminescence and morpho-structural characteristics of phosphor powders. In this respect different mineralising agents such as sodium/lithium carbonate, sodium tetraborate ans sodium pyrophosphate were used during the thermal synthesis stage. Thermal analysis, X-ray diffraction, scanning electron microscopy, infrared spectroscopy and photoluminescence measurements were used to investigate precursor and phosphor powders. The correlation between the phosphor properties and precursor quality enabled us to select the optimal synthesis conditions. (C) 2008 Elsevier B.V. All rights reserved.
引用
收藏
页码:346 / 349
页数:4
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