Hydrostatic low-range pressure applications of the Paris-Edinburgh cell utilizing polymer gaskets for diffuse X-ray scattering measurements

被引：10

作者：

Chapman, Karena W. ^{[1
]}

Chupas, Peter J.

Kurtz, Charles A.

Locke, Darren R.

Parise, John B.

Hriljac, Joseph A.

机构：

[1] Argonne Natl Lab, Adv Photon Source, Xray Sci Div, Argonne, IL 60439 USA

[2] SUNY Stony Brook, Dept Geosci, Stony Brook, NY 11794 USA

[3] Univ Birmingham, Sch Chem, Birmingham B15 2TT, W Midlands, England

来源：

JOURNAL OF APPLIED CRYSTALLOGRAPHY | 2007年 / 40卷

关键词：

D O I：

10.1107/S0021889806047923

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The use of a polymeric Torlon (polyamide-imide) gasket material in a Paris Edinburgh pressure cell for in situ high-pressure X-ray scattering measurements is demonstrated. The relatively low bulk modulus of the gasket allows for fine control of the sample pressure over the range 0.01-0.42 GPa. The quality of the data obtained in this way is suitable for Bragg and pair distribution function analysis.

引用

页码：196 / 198

页数：3

共 13 条

[1] NEUTRON POWDER DIFFRACTION ABOVE 10-GPA [J].

BESSON, JM ;

NELMES, RJ ;

HAMEL, G ;

LOVEDAY, JS ;

WEILL, G ;

HULL, S .

PHYSICA B, 1992, 180 :907-910

[2] Rapid-acquisition pair distribution function (RA-PDF) analysis [J].

Chupas, PJ ;

Qiu, XY ;

Hanson, JC ;

Lee, PL ;

Grey, CP ;

Billinge, SJL .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2003, 36 :1342-1347

[3] HIGH-PRESSURE EQUATION OF STATE FOR NACL, KCL, AND CSCL [J].

DECKER, DL .

JOURNAL OF APPLIED PHYSICS, 1971, 42 (08) :3239-&

[4] Strain-induced crystallisation in bulk amorphous PET under uni-axial loading [J].

Gorlier, E ;

Haudin, JM ;

Billon, N .

POLYMER, 2001, 42 (23) :9541-9549

[5]

Hammersley A. P., 1997, ESRF97HA02T

[6] Two-dimensional detector software: From real detector to idealised image or two-theta scan [J].

Hammersley, AP ;

Svensson, SO ;

Hanfland, M ;

Fitch, AN ;

Hausermann, D .

HIGH PRESSURE RESEARCH, 1996, 14 (4-6) :235-248

[7] A new type of compact large-capacity press for neutron and X-ray scattering [J].

Klotz, S ;

Hamel, G ;

Frelat, J .

HIGH PRESSURE RESEARCH, 2004, 24 (01) :219-223

[8]

Larson A. C., 1987, LAUR86748 LOS AL NAT

[9] Attainment of near-hydrostatic compression conditions using the Paris-Edinburgh cell [J].

Marshall, WG ;

Francis, DJ .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2002, 35 :122-125

[10] Quantitative high-pressure pair distribution function analysis of nanocrystalline gold [J].

Martin, CD ;

Antao, SM ;

Chupas, PJ ;

Lee, PL ;

Shastri, SD ;

Parise, JB .

APPLIED PHYSICS LETTERS, 2005, 86 (06) :1-3

← 1 2 →