Structural determination of quercusides A and B, new flavonoid glucosides from Quercus incana, by 1D and 2D NMR spectroscopy

被引:2
作者
Iftikhar, Benish [2 ]
Perveen, Shagufta [1 ]
Malik, Abdul [1 ]
Sultana, Najma [3 ]
Arayne, Saeed [2 ]
Muhammad, Pir [4 ]
机构
[1] Univ Karachi, HEJ Res Inst Chem, Int Ctr Chem & Biol Sci, Karachi 75270, Pakistan
[2] Univ Karachi, Dept Chem, Karachi 75270, Pakistan
[3] Univ Karachi, Fac Pharm, Dept Pharmaceut Chem, Karachi 75270, Pakistan
[4] Jahanzeb Postgrad Coll, Dept Chem, Saidu Sharif, Swat, Pakistan
关键词
NMR; H-1; C-13; quercuside A; quercuside B; flavonoids; Quercus incana;
D O I
10.1002/mrc.2426
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Quercusides A and B, new flavonoid glucosides have been isolated from the chloroform soluble fractions of Quercus incana. Their structures were assigned from H-1 and C-13 nuclear magnetic resonance spectra, distortionless enhancement by polarization transfer (DEPT) and by correlation spectroscopy, heteronuclear multiple quantum correlation (HMQC) and heteronuclear multiple bond correlation (HMBC) experiments. Lupeol, beta-sitosterol and ursolic acid have also been reported from this species. Copyright (c) 2009 John Wiley & Sons, Ltd.
引用
收藏
页码:605 / 608
页数:4
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